commiss regul ec februari lai method sampl analysi offici control level mycotoxin foodstuff text eea relev commiss european commun regard treati establish european commun regard regul ec european parliament council april offici control perform ensur verif complianc feed food law anim health anim welfar rule articl commiss regul ec march set maximum level contamin foodstuff maximum limit mycotoxin foodstuff sampl plai crucial part precis determin level mycotoxin heterogen distribut lot fix gener criteria sampl method compli fix gener criteria method analysi compli order ensur control laboratori method analysi compar level perform commiss direct ec juli lai sampl method method analysi offici control level contamin foodstuff establish sampl method perform criteria method analysi offici control level aflatoxin foodstuff commiss direct ec march lai sampl method method analysi offici control level ochratoxin foodstuff commiss direct ec august lai sampl method method analysi offici control level patulin foodstuff commiss direct ec june lai sampl method method analysi offici control level fusarium toxin foodstuff similarli establish sampl method perform criteria ochratoxin patulin fusarium toxin appli sampl method product control mycotoxin sampl method perform criteria method analysi offici control mycotoxin brought singl legal act order make easier appli aflatoxin heterogen distribut lot lot food product larg particl size dri fig groundnut order obtain repres batch food product larg particl size weight aggreg sampl larger case batch food product smaller particl size distribut mycotoxin process product gener heterogen unprocess cereal product provid simpler sampl provis process product direct ec ec ec ec repeal date applic regul coincid date applic commiss regul ec june amend regul ec fusarium toxin measur provid regul accord opinion stand committe food chain anim health adopt regul articl sampl offici control level mycotoxin foodstuff carri accord method set annex articl sampl prepar method analysi offici control level mycotoxin foodstuff compli criteria set annex ii articl direct ec ec ec ec repeal refer repeal direct constru refer regul articl regul enter forc dai public offici journal european union appli juli regul bind entireti directli applic member state brussel februari commiss marko kyprian member commiss oj correct oj oj regul amend regul ec oj oj direct amend direct ec oj oj direct amend direct ec oj oj oj oj annex method sampl offici control level mycotoxin foodstuff gener provis offici control perform accord provis regul ec gener provis appli prejudic provis regul ec purpos scope sampl intend offici control level mycotoxin content foodstuff method set annex aggreg sampl obtain consid repres lot complianc maximum limit laid regul ec establish basi level determin laboratori sampl definit purpos annex definit appli quot lot quot mean identifi quantiti food commod deliv time determin offici common characterist origin varieti type pack packer consignor mark quot sublot quot mean design part larg lot order appli sampl method design part sublot physic separ identifi quot increment sampl quot mean quantiti materi singl place lot sublot quot aggreg sampl quot mean combin total increment sampl lot sublot quot laboratori sampl quot mean sampl intend laboratori gener provis personnel sampl perform authoris person design member state materi sampl lot examin sampl separ accord specif sampl provis mycotoxin larg lot subdivid sublot sampl separ precaut sampl prepar sampl precaut avoid affect mycotoxin content advers affect analyt determin make aggreg sampl unrepres food safeti lot sampl measur ensur safeti person take sampl increment sampl increment sampl place distribut lot sublot departur procedur record record provid part annex prepar aggreg sampl aggreg sampl made combin increment sampl replic sampl replic sampl enforc trade defenc refer refere purpos homogenis aggreg sampl procedur conflict member state rule right food busi oper packag transmiss sampl sampl clean inert contain offer adequ protect contamin damag transit precaut avoid chang composit sampl aris transport storag seal label sampl sampl offici seal place sampl identifi rule member state record sampl permit lot identifi unambigu give date place sampl addit inform assist analyst type lot food commod trade bulk contain individu pack sack bag retail pack method sampl appli form commod put market prejudic specif provis set part annex formula guid sampl lot trade individu pack sack bag retail pack weight kg sampl frequenc sf nth sack bag increment sampl decim figur round nearest number method sampl cereal cereal product method sampl applic offici control maximum level establish aflatoxin total aflatoxin ochratoxin fusarium toxin cereal cereal product weight increment sampl weight increment sampl gram defin part annex case lot retail pack weight increment sampl depend weight retail pack case retail pack gram result aggreg sampl weigh kg weight singl retail pack gram gram individu retail pack increment sampl sampl laboratori case method sampl lead unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli case valuabl product market retail pack gram kg aggreg sampl obtain aggreg number increment sampl smaller number tabl condit weight aggreg sampl equal requir weight aggreg sampl mention tabl retail pack gram differ larg retail pack consid increment sampl result aggreg sampl kg weight retail pack gram increment sampl consist retail pack gram approxim close gener survei method sampl cereal cereal product tabl subdivis lot sublot depend product lot weight commod lot weight tonn weight number sublot number increment sampl aggreg sampl weight kg cereal cereal product tonn gt lt sublot tonn lt method sampl cereal cereal product lot tonn condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum case lot physic separ sublot minimum increment sampl lot sublot sampl separ number increment sampl weight aggreg sampl kg carri method sampl set point unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document altern method sampl appli case practic imposs appli abovement method sampl case larg lot cereal store warehous cereal store silo method sampl cereal cereal product lot lt tonn lot cereal cereal product tonn sampl plan increment sampl depend lot weight result aggreg sampl kg small lot tonn lower number increment sampl aggreg sampl combin increment sampl case kg figur tabl determin number increment sampl tabl number increment sampl depend weight lot cereal cereal product lot weight tonn number increment sampl aggreg sampl weight kg gt gt gt gt gt gt sampl retail stage sampl foodstuff retail stage accord provis set part annex altern method sampl retail stage appli provid ensur aggreg sampl suffici repres sampl lot fulli document case aggreg sampl kg accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl dri fruit includ dri vine fruit deriv product except dri fig method sampl applic offici control maximum level establish aflatoxin total aflatoxin dri fruit except dri fig ochratoxin dri vine fruit currant raisin sultana weight increment sampl weight increment sampl gram defin part annex case lot retail pack weight increment sampl depend weight retail pack case retail pack gram result aggreg sampl weigh kg weight singl retail pack gram gram individu retail pack increment sampl sampl laboratori case method sampl lead unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli case valuabl product market retail pack gram kg aggreg sampl obtain aggreg number increment sampl smaller number tabl condit weight aggreg sampl correspond requir weight aggreg sampl mention tabl retail pack gram differ larg retail pack consid increment sampl result aggreg sampl kg weight retail pack gram increment sampl consist retail pack gram approxim close gener survei method sampl dri fruit except fig tabl subdivis lot sublot depend product lot weight commod lot weight tonn weight number sublot number increment sampl aggreg sampl weight kg dri fruit tonn lt method sampl dri fruit lot tonn except fig condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum sublot sampl separ number increment sampl weight aggreg sampl kg carri method sampl commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document method sampl dri fruit lot lt tonn except fig dri fruit lot except fig tonn sampl plan increment sampl depend lot weight result aggreg sampl kg figur tabl determin number increment sampl tabl number increment sampl depend weight lot dri fruit lot weight tonn number increment sampl aggreg sampl weight kg gt gt gt gt gt gt gt sampl retail stage sampl foodstuff retail stage accord provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document case aggreg sampl kg specif sampl provis dri fruit except dri fig trade vacuum pack lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight correspond weight sampl lot tabl accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl dri fig groundnut nut method sampl applic offici control maximum level establish aflatoxin total aflatoxin dri fig groundnut nut weight increment sampl weight increment sampl gram defin part annex case lot retail pack weight increment sampl depend weight retail pack case retail pack gram result aggreg sampl weigh kg weight singl retail pack gram gram individu retail pack increment sampl sampl laboratori case method sampl lead unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli case valuabl product market retail pack gram kg aggreg sampl obtain aggreg number increment sampl smaller number tabl condit weight aggreg sampl correspond requir weight aggreg sampl mention tabl retail pack gram differ larg retail pack consid increment sampl result aggreg sampl kg weight retail pack gram increment sampl consist retail pack gram approxim close gener survei method sampl dri fig groundnut nut tabl subdivis lot sublot depend product lot weight commod lot weight tonn weight number sublot number increment sampl aggreg sampl weight kg dri fig tonn lt groundnut pistachio brazil nut nut tonn gt lt sublot tonn lt method sampl dri fig groundnut nut lot tonn condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum sublot sampl separ number increment sampl weight aggreg sampl kg mix divid equal laboratori sampl kg grind divis laboratori sampl case groundnut nut subject sort physic treatment avail equip homogenis kg sampl laboratori sampl kg separ ground fine mix achiev complet homogenis accord provis laid annex ii carri method sampl commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document method sampl dri fig groundnut nut lot lt tonn number increment sampl depend weight lot minimum maximum figur tabl determin number increment sampl subsequ divis aggreg sampl tabl number increment sampl depend weight lot number subdivis aggreg sampl lot weight tonn number increment sampl aggreg sampl weight kg case retail pack weight aggreg sampl diverg point number laboratori sampl aggreg sampl divis gt divis gt divis gt lt kg divis gt gt lt kg gt gt weight aggreg sampl kg mix divid equal laboratori sampl kg grind divis laboratori sampl case dri fig groundnut nut subject sort physic treatment avail equip homogenis kg sampl case aggreg sampl weight kg aggreg sampl divid laboratori sampl guidanc lt kg divis laboratori sampl lt kg divis laboratori sampl kg divis laboratori sampl laboratori sampl separ ground fine mix achiev complet homogenis accord provis laid annex ii carri method sampl unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document method sampl deriv product compound food deriv product small particl weight flour peanut butter homogen distribut aflatoxin contamin number increment sampl lot tonn number increment sampl depend lot weight tabl tabl number increment sampl depend weight lot lot weight tonn number increment sampl aggreg sampl weight kg gt gt gt gt weight increment sampl gram case lot retail pack weight increment sampl depend weight retail pack weight aggreg sampl kg suffici mix deriv product larg particl size heterogen distribut aflatoxin contamin method sampl accept dri fig groundnut nut sampl retail stage sampl foodstuff retail stage accord provis set part annex effect method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document case aggreg sampl kg specif method sampl groundnut nut dri fig deriv product trade vacuum pack pistachio groundnut brazil nut dri fig lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight correspond weight sampl lot tabl nut pistachio brazil nut lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight equal weight sampl lot tabl product deriv nut fig groundnut small particl size lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight correspond weight sampl lot tabl accept lot sublot dri fig groundnut nut subject sort physic treatment accept aggreg sampl averag laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject aggreg sampl averag laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti dri fig groundnut nut intend direct human consumpt accept laboratori sampl exce maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti case aggreg sampl kg accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl spice method sampl applic offici control maximum level establish aflatoxin total aflatoxin spice weight increment sampl weight increment sampl gram defin part annex case lot retail pack weight increment sampl depend weight retail pack case retail pack gt gram result aggreg sampl weigh kg weight singl retail pack gt gt gram gram individu retail pack increment sampl sampl laboratori case method sampl lead unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli case valuabl product market retail pack gram kg aggreg sampl obtain aggreg number increment sampl smaller number tabl condit weight aggreg sampl correspond requir weight aggreg sampl mention tabl retail pack gram differ larg retail pack consid increment sampl result aggreg sampl kg weight retail pack gram increment sampl consist retail pack gram approxim close gener survei method sampl spice tabl subdivis lot sublot depend product lot weight commod lot weight tonn weight number sublot number increment sampl aggreg sampl weight kg spice tonn lt method sampl spice lot tonn condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum sublot sampl separ number increment sampl weight aggreg sampl kg carri method sampl unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document method sampl spice lot lt tonn lot spice tonn sampl plan increment sampl depend lot weight result aggreg sampl kg figur tabl determin number increment sampl tabl number increment sampl depend weight lot spice lot weight tonn number increment sampl aggreg sampl weight kg gt gt gt gt gt gt gt gt sampl retail stage sampl foodstuff retail stage accord sampl provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document case aggreg sampl kg specif method sampl spice trade vacuum pack lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight correspond weight sampl lot tabl accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl milk milk product infant formula follow formula includ infant milk follow milk method sampl applic offici control maximum level establish aflatoxin milk milk product infant formula follow formula includ infant milk follow milk dietari food milk milk product special medic purpos intend specif infant method sampl milk milk product infant formula follow formula includ infant milk follow milk aggreg sampl kg litr sampl consist bottl minimum number increment sampl lot tabl number increment sampl determin function usual form product concern commercialis case bulk liquid product lot mix affect qualiti product manual mechan mean immedi prior sampl case homogen distribut aflatoxin assum lot suffici increment sampl lot form aggreg sampl increment sampl frequent bottl packag similar weight weight increment sampl gram result aggreg sampl kg litr departur method record record provid part annex tabl minimum number increment sampl lot form commercialis volum weight lot litr kg minimum number increment sampl minimum volum weight aggreg sampl litr kg bulk bottl packag bottl packag bottl packag gt sampl retail stage sampl foodstuff retail stage accord provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti decis limit annex ii point reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti decis limit annex ii point method sampl coffe coffe product method sampl applic offici control maximum level establish ochratoxin roast coffe bean ground roast coffe solubl coffe weight increment sampl weight increment sampl gram defin part annex case lot retail pack weight increment sampl depend weight retail pack case retail pack gram result aggreg sampl weigh kg weight singl retail pack gram gram individu retail pack increment sampl sampl laboratori case method sampl lead unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli case valuabl product market retail pack gram kg aggreg sampl obtain aggreg number increment sampl smaller number tabl condit weight aggreg sampl correspond requir weight aggreg sampl mention tabl retail pack gram differ larg retail pack consid increment sampl result aggreg sampl kg weight retail pack gram increment sampl consist retail pack gram approxim close gener survei method sampl roast coffe tabl subdivis lot sublot depend product lot weight commod lot weight tone weight number sublot number increment sampl aggreg sampl weight kg roast coffe bean ground roast coffe solubl coffe tonn lt method sampl roast coffe bean ground roast coffe solubl coffe lot tonn condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot vari mention weight maximum sublot sampl separ number increment sampl weight aggreg sampl kg carri method sampl unaccept commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document method sampl roast coffe bean ground roast coffe solubl coffe lot lt tonn roast coffe bean ground roast coffe solubl coffe tonn sampl plan increment sampl depend lot weight result aggreg sampl kg figur tabl determin number increment sampl tabl number increment sampl depend weight lot roast coffe bean ground roast coffe solubl coffe lot weight tonn number increment sampl aggreg sampl weight kg gt gt gt gt gt gt gt method sampl roast coffe bean ground roast coffe solubl coffe trade vacuum pack lot equal tonn increment sampl result kg aggreg sampl lot tonn number increment sampl mention tabl result aggreg sampl weight correspond weight sampl lot tabl sampl retail stage sampl foodstuff retail stage accord sampl provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document case aggreg sampl kg accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl fruit juic includ grape juic grape cider wine method sampl applic offici control maximum level establish ochratoxin wine grape juic grape patulin fruit juic fruit nectar spirit drink cider ferment drink deriv appl appl juic method sampl aggreg sampl litr sampl consist bottl minimum number increment sampl lot tabl number increment sampl determin function usual form product concern commercialis case bulk liquid product lot mix affect qualiti product manual mechan mean immedi prior sampl case homogen distribut ochratoxin patulin assum lot suffici increment sampl lot form aggreg sampl increment sampl frequent bottl packag similar weight weight increment sampl gram result aggreg sampl litr departur method record record provid part annex tabl minimum number increment sampl lot form commercialis volum lot litr minimum number increment sampl minimum volum aggreg sampl litr bulk fruit juic spirit drink cider wine bottl packag fruit juic spirit drink cider bottl packag fruit juic spirit drink cider bottl packag fruit juic spirit drink cider gt bottl packag wine bottl packag wine bottl packag wine gt sampl retail stage sampl foodstuff retail stage accord provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti method sampl solid appl product appl juic solid appl product infant young children method sampl applic offici control maximum level establish patulin solid appl product appl juic solid appl product infant young children method sampl aggreg sampl kg sampl singl packag minimum number increment sampl lot tabl case liquid product lot mix manual mechan mean immedi prior sampl case homogen distribut patulin assum lot suffici increment sampl lot form aggreg sampl increment sampl similar weight weight increment sampl gram result aggreg sampl kg departur method record record provid part annex tabl minimum number increment sampl lot weight lot kg minimum number increment sampl aggreg sampl weight kg lt gt lot consist individu packag number packag form aggreg sampl tabl tabl number packag increment sampl form aggreg sampl lot consist individu packag number packag unit lot number packag unit aggreg sampl weight kg packag unit packag unit gt maximum packag unit sampl retail stage sampl foodstuff retail stage accord sampl provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document accept lot sublot accept laboratori sampl conform maximum limit take account measur uncertainti correct recoveri reject laboratori sampl exce maximum limit reason doubt take account measur uncertainti correct recoveri method sampl babi food process cereal base food infant young children method sampl applic offici control maximum level establish aflatoxin ochratoxin fusarium toxin babi food process cereal base food infant young children aflatoxin ochratoxin dietari food special medic purpos milk milk product intend specif infant patulin babi food process cereal base food infant young children control maximum level establish patulin appl juic solid appl product infant young children method sampl part annex appli method sampl method sampl cereal cereal product set point annex appli food intend infant young children number increment sampl depend weight lot minimum maximum accord tabl point annex small lot tonn lower number increment sampl aggreg sampl unit increment sampl case kg weight increment sampl gram case lot retail pack weight increment sampl depend weight retail pack case small lot tonn increment sampl weight unit increment sampl result aggreg sampl kg departur method record record provid weight aggreg sampl kg suffici mix sampl retail stage sampl foodstuff retail stage accord provis set part annex altern method sampl retail stage provid ensur aggreg sampl suffici repres sampl lot fulli document accept lot sublot accept laboratori sampl conform maximum limit take account correct recoveri measur uncertainti reject laboratori sampl exce maximum limit reason doubt take account correct recoveri measur uncertainti guidanc document compet author control complianc eu legisl aflatoxin http europa eu int comm food food chemicalsafeti contamin aflatoxin guidanc en pdf guidanc document addit practic inform inform contain guidanc document subordin provis regul depend lot weight tabl guidanc sampl lot provid guidanc document juli onward websit http europa eu int comm food food chemicalsafeti contamin index en htm case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg depend lot weight tabl part annex case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg depend lot weight tabl part annex case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg depend lot weight tabl part annex case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg depend lot weight tabl annex case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg case portion sampl small imposs obtain aggreg sampl litr aggreg sampl volum litr case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg case portion sampl small imposs obtain aggreg sampl kg aggreg sampl weight kg annex ii criteria sampl prepar method analysi offici control level mycotoxin foodstuff introduct precaut distribut mycotoxin gener homogen sampl prepar homogenis extrem care complet sampl receiv laboratori homogen case homogenis perform laboratori analysi aflatoxin daylight exclud procedur aflatoxin gradual break influenc ultra violet light calcul proport shell kernel nut limit fix aflatoxin regul ec appli edibl part level aflatoxin edibl part determin sampl nut quot shell quot shell level aflatoxin determin edibl part nut quot shell quot sampl prepar procedur method sampl analysi estim weight nut kernel aggreg sampl weight nut kernel aggreg sampl estim establish suitabl factor proport nut shell nut kernel nut proport ascertain amount kernel bulk sampl sampl prepar method analysi approxim nut random separ lot put aggreg sampl ratio laboratori sampl obtain weigh nut shell weigh shell kernel portion proport shell kernel establish laboratori number sampl assum futur analyt work laboratori sampl found contravent limit proport determin sampl approxim nut set treatment sampl receiv laboratori laboratori sampl fine grind mix process demonstr achiev complet homogenis case maximum level appli dry matter dry matter content product determin part homogenis sampl method demonstr determin accur dry matter content replic sampl replic sampl enforc trade defenc refer refere purpos homogenis materi procedur conflict member state rule right food busi oper method analysi laboratori laboratori control requir definit number commonli definit laboratori requir repeat absolut differ singl test result obtain repeat condit sampl oper apparatu laboratori short interv time expect lie specif probabl typic sr sr standard deviat calcul result gener repeat condit tiff rsdr rel standard deviat calcul result gener repeat condit sr reproduc absolut differ singl test result obtain reproduc condit ident materi obtain oper laboratori standardis test method expect lie probabl typic sr sr standard deviat calcul result reproduc condit tiff rsdr rel standard deviat calcul result gener reproduc condit sr gener requir method analysi food control purpos compli provis item annex iii regul ec specif requir perform criteria specif method determin mycotoxin level foodstuff requir commun legisl laboratori select method provid select method meet criteria perform criteria aflatoxin note valu appli sum sum individu aflatoxin report respons analyt system equival criterion concentr rang recommend maximum permit blank neglig recoveri aflatoxin μg kg gt μg kg recoveri aflatoxin lt μg kg μg kg gt μg kg precis rsdr deriv horwitz equat deriv horwitz equat precis rsdr calcul time precis rsdr concentr interest perform criteria ochratoxin level μg kg ochratoxin rsdr rsdr recoveri lt perform criteria patulin level μg kg patulin rsdr rsdr recoveri lt gt perform criteria deoxynivalenol level μg kg deoxynivalenol rsdr rsdr recoveri gt gt perform criteria zearalenon level μg kg zearalenon rsdr rsdr recoveri gt perform criteria fumonisin level μg kg fumonisin rsdr rsdr recoveri gt perform criteria ht toxin level μg kg toxin rsdr rsdr recoveri gt level μg kg ht toxin rsdr rsdr recoveri gt note perform criteria mycotoxin detect limit method state precis valu concentr interest precis valu calcul horwitz equat rsdr logc tiff rsdr rel standard deviat calcul result gener reproduc condit sr concentr ratio mg kg generalis precis equat found independ analyt matrix sole depend concentr routin method analysi quot fit purpos quot approach case limit number fulli valid method analysi altern quot fit purpos quot approach defin singl paramet fit function evalu accept method analysi fit function uncertainti function specifi maximum level uncertainti regard fit purpos limit number method analysi fulli valid collabor trial determin ht toxin uncertainti function approach maximum accept uncertainti assess suitabl quot fit purpos quot method analysi laboratori laboratori method produc result maximum standard uncertainti maximum standard uncertainti calcul formula uf maximum standard uncertainti μg kg lod limit detect method μg kg constant numer factor depend valu set tabl concentr interest μg kg analyt method result uncertainti measur maximum standard uncertainti method consid equal suitabl meet perform criteria point tabl numer valu constant formula set point depend concentr interest μg kg gt estim measur uncertainti recoveri calcul report result analyt result report correct uncorrect recoveri manner report level recoveri report analyt result correct recoveri control complianc analyt result report analyt result expand measur uncertainti expand measur uncertainti coverag factor level confid approxim food anim origin take account measur uncertainti establish decis limit ccα accord commiss decis ec point annex case substanc establish permit limit present interpret rule analyt result view accept reject lot appli analyt result obtain sampl offici control case analysi defenc refere purpos nation rule appli laboratori qualiti standard laboratori compli provis articl regul ec offici control perform ensur verif complianc feed food law anim health anim welfar rule detail procedur estim measur uncertainti procedur assess recoveri found report quot report relationship analyt result measur uncertainti recoveri factor provis eu food feed legisl quot http europa eu int comm food food chemicalsafeti contamin report sampl analysi en pdf oj decis amend decis ec oj transit arrang provid articl commiss regul ec decemb lai transit arrang implement regul ec european parliament council amend regul ec oj