commiss direct ec august lai sampl method method analysi offici control level patulin foodstuff text eea relev commiss european commun regard treati establish european commun regard council direct eec decemb introduct commun method sampl analysi monitor foodstuff intend human consumpt articl thereof commiss regul ec march set maximum level contamin foodstuff amend commiss regul ec fix maximum limit patulin foodstuff council direct eec octob subject addit measur offici control foodstuff introduc system qualiti standard laboratori entrust member state offici control foodstuff fix gener criteria method analysi compli order ensur laboratori charg control method analysi compar level perform major import analyt result report interpret uniform order ensur harmonis enforc approach european union interpret rule applic analyt result obtain sampl offici control case analysi defenc refere purpos nation rule appli provis sampl method analysi drawn basi present knowledg adapt account advanc scientif technolog knowledg measur provid direct accord opinion stand committe food chain anim health adopt direct articl member state measur ensur sampl offici control level patulin foodstuff carri accord method annex direct articl member state measur ensur sampl prepar method analysi offici control level patulin foodstuff compli criteria annex ii direct articl member state bring forc law regul administr provis compli direct septemb latest forthwith inform commiss thereof member state adopt provis refer direct accompani refer occas offici public member state determin refer made member state commun commiss text provis nation law adopt field govern direct articl direct enter forc dai public offici journal european union articl direct address member state brussel august commiss david byrn member commiss oj oj page offici journal oj annex method sampl offici control level patulin foodstuff purpos scope sampl intend offici check level patulin foodstuff method aggreg sampl obtain consid repres lot complianc maximum level laid commiss regul ec establish basi level determin laboratori sampl definit gt tabl gt gener provis personnel sampl perform authoris person member state materi sampl lot examin sampl separ precaut sampl prepar sampl precaut avoid affect patulin content advers affect analyt determin make aggreg sampl unrepres increment sampl increment sampl place distribut lot sublot departur procedur record record prepar aggreg sampl aggreg sampl made unit increment sampl kg practic singl packag sampl replic sampl replic sampl enforc trade defenc refere purpos homogenis aggreg sampl conflict member state rule sampl packag transmiss sampl sampl clean inert contain offer adequ protect contamin damag transit precaut avoid chang composit sampl aris transport storag seal label sampl sampl offici seal place sampl identifi member state regul record sampl permit lot identifi unambigu give date place sampl addit inform assist analyst sampl plan sampl method appli ensur aggreg sampl repres lot control number increment sampl aggreg sampl kg point sampl singl packag minimum number increment sampl lot tabl case liquid product lot mix manual mechan mean immedi prior sampl case homogen distribut patulin assum lot suffici increment sampl lot form aggreg sampl increment sampl similar weight weight increment sampl gram result aggreg sampl kg departur procedur record record provid tabl minimum number increment sampl lot gt tabl gt lot consist individu packag number packag form aggreg sampl tabl tabl number packag increment sampl form aggreg sampl lot consist individu packag gt tabl gt complianc lot sublot specif control laboratori analys laboratori sampl enforc duplic analysi case obtain result analysi maximum level calcul result lot accept result analysi maximum level duplic analysi exce respect maximum level laid regul ec take account measur uncertainti correct recoveri lot compliant maximum level laid regul ec correct recoveri exce maximum level reason doubt take account measur uncertainti annex ii sampl prepar criteria method analysi offici check level patulin foodstuff precaut distribut patulin foodstuff homogen sampl prepar homogenis extrem care materi receiv laboratori prepar test materi treatment sampl receiv laboratori fine grind relev mix complet aggreg sampl process demonstr achiev complet homogenis subdivis sampl enforc defenc purpos replic sampl enforc trade defenc refere purpos homogenis materi conflict member state rule sampl method analysi laboratori laboratori control requir definit number commonli definit laboratori requir commonli quot precis paramet repeat reproduc repeat absolut differ singl test result obtain repeat condit sampl oper apparatu laboratori short interv time expect lie specif probabl typic sr sr standard deviat calcul result gener repeat condit rsdr rel standard deviat calcul result gener repeat condit gt refer graphic gt gt refer graphic gt averag result laboratori sampl reproduc absolut differ singl test result obtain reproduc condit ident materi obtain oper laboratori standardis test method expect lie probabl typic sr sr standard deviat calcul result reproduc condit rsdr rel standard deviat calcul result gener reproduc condit gt refer graphic gt gener requir method analysi food control purpos compli provis item annex council direct eec decemb introduct commun method sampl analysi monitor foodstuff intend human consumpt specif requir specif method determin patulin foodstuff prescrib commun level laboratori select method provid select method meet criteria perform characterist patulin gt tabl gt detect limit method state precis valu concentr interest precis valu calcul horwitz equat gt refer graphic gt rsdr rel standard deviat calcul result gener reproduc condit gt refer graphic gt concentr ratio mg kg generalis precis equat found independ analyt matrix sole depend concentr routin method analysi recoveri calcul report result analyt result report correct uncorrect recoveri manner report level recoveri report analyt result correct recoveri check complianc annex point analyt result report analyt result measur uncertainti laboratori qualiti standard laboratori compli council direct eec octob subject addit measur offici control foodstuff oj