commiss direct ec march lai sampl method method analysi offici control level lead cadmium mercuri mcpd foodstuff text eea relev commiss european commun regard treati establish european commun regard council direct eec decemb introduct commun method sampl analysi monitor foodstuff intend human consumpt articl thereof council regul eec februari lai commun procedur contamin food maximum level set contamin foodstuff order protect public health commiss regul ec march set maximum level contamin foodstuff establish maximum level lead cadmium mercuri monochloropropan diol mcpd foodstuff make refer measur lai sampl analysi method council direct eec june offici control foodstuff lai gener principl perform control foodstuff council direct eec octob subject addit measur offici control foodstuff introduc system qualiti standard laboratori entrust member state offici control foodstuff sampl plai crucial role obtain repres result determin level contamin heterogen distribut lot direct eec fix gener criteria method sampl analysi case specif criteria order ensur laboratori charg control method analysi compar level perform provis sampl method analysi drawn basi present knowledg adapt account advanc scientif technolog knowledg measur provid direct accord opinion stand committe foodstuff adopt direct articl member state measur ensur sampl offici control level lead cadmium mercuri mcpd foodstuff carri accord method annex direct articl member state measur ensur sampl prepar method analys offici control level lead cadmium mercuri mcpd foodstuff compli criteria annex ii direct articl member state april bring forc law regul administr provis compli provis direct forthwith notifi commiss thereof member state adopt provis provis refer direct accompani refer time offici public procedur refer adopt member state articl direct enter forc dai public offici journal european commun direct address member state brussel march commiss david byrn member commiss oj oj page offici journal oj oj annex method sampl offic control level lead cadmium mercuri mcpd foodstuff purpos scope sampl intend offici control level lead cadmium mercuri mcpd content foodstuff method aggreg sampl obtain consid repres lot sublot complianc maximum level laid regul ec establish basi level determin laboratori sampl definit gt tabl gt gener provis personnel sampl perform authoris qualifi person member state materi sampl lot examin sampl separ precaut sampl prepar laboratori sampl precaut avoid affect lead cadmium mercuri mcpd content advers affect analyt determin make aggreg sampl unrepres increment sampl increment sampl place distribut lot sublot departur procedur record record provid prepar aggreg sampl aggreg sampl made unit increment sampl kg practic singl packag sampl subdivis aggreg sampl laboratori sampl enforc defenc refere purpos laboratori sampl enforc trade defenc refere purpos homogenis aggreg sampl conflict member state regul sampl size laboratori sampl enforc suffici duplic analys packag transmiss aggreg laboratori sampl aggreg laboratori sampl clean inert contain offer adequ protect contamin loss analyt adsorpt intern wall contain damag transit precaut avoid chang composit aggreg laboratori sampl aris transport storag seal label aggreg laboratori sampl sampl offici seal place sampl identifi member state regul record sampl permit lot identifi unambigu give date place sampl addit inform assist analyst sampl plan sampl ideal place point commod enter food chain discret lot identifi sampl method appli ensur aggreg sampl repres lot control number increment sampl case liquid product homogen distribut contamin question assum lot suffici increment sampl lot form aggreg sampl refer lot number liquid product hydrolys veget protein hvp liquid soya sauc shaken homogenis suitabl mean increment sampl product minimum number increment sampl lot tabl increment sampl similar weight departur procedur record record provid tabl minimum number increment sampl lot gt tabl gt lot consist individu packag number packag form aggreg sampl tabl tabl number packag increment sampl form aggreg sampl lot consist individu packag gt tabl gt complianc lot sublot specif control laboratori analys laboratori sampl enforc independ analys calcul result lot accept conform respect maximum level laid regul ec reject exce respect maximum level annex ii sampl prepar criteria method analysi offic control level lead cadmium mercuri mcpd foodstuff introduct basic requir obtain repres homogen laboratori sampl introduc secondari contamin specif sampl prepar procedur lead cadmium mercuri satisfactori specif sampl prepar procedur product consider draft cen standard quot foodstuff determin trace element perform criteria gener consider quot found satisfactori equal valid point note procedur bivalv mollusc crustacean small fish eaten viscera includ materi analys veget edibl portion test note requir regul ec method analysi laboratori laboratori control requir definit gt tabl gt gener requir method analysi food control purpos compli provis paragraph annex direct eec analysi lead wine commiss regul eec determin commun method analysi wine lai method chapter annex specif requir lead cadmium mercuri analys specif method determin lead cadmium mercuri content prescrib laboratori valid method fulfil perform criteria tabl valid includ certifi refer materi collabor trial test materi tabl perform criteria method lead cadmium mercuri analys gt tabl gt mcpd analysi specif method determin mcpd content prescrib laboratori valid method fulfil perform criteria tabl valid includ certifi refer materi collabor trial test materi specif method valid collabor trial shown meet requir tabl tabl perform criteria method mcpd analysi gt tabl gt estim analyt trueness recoveri calcul trueness analysi estim includ suitabl certifi refer materi analyt run quot harmonis guidelin recoveri inform analyt measur quot develop auspic iupac iso aoac account analyt result report correct uncorrect manner report level recoveri report laboratori qualiti standard laboratori compli direct eec express result result express unit maximum level laid regul ec refer draft standard pren quot foodstuff determin trace element perform criteria gener consider quot cen rue de stassart brussel horwitz quot evalu analyt method regul food drug quot anal chem method analysi determin monochloropropan diol food food ingredi mass spectrometr detect submit cen tc aoac intern quot report scientif cooper task provis valid method support scientif committe food recommend mcpd hydrolys protein food quot iso aoac iupac harmonis guidelin recoveri inform analyt measur edit michael thompson steven ellison al fajgelj paul willett roger wood pure appl chem oj