commiss direct ec juli lai sampl method method analysi offici control level contamin foodstuff text eea relev commiss european commun regard treati establish european commun regard council direct eec decemb introduct commun method sampl analysi monitor foodstuff intend human consumpt articl thereof commiss regul ec juli amend commiss regul ec set maximum level contamin foodstuff fix maximum limit aflatoxin foodstuff council direct eec octob subject addit measur offici control foodstuff introduc system qualiti standard laboratori entrust member state offici control foodstuff sampl plai crucial part precis determin level aflatoxin heterogen distribut lot fix gener criteria method analysi compli order ensur laboratori charg control method analysi compar level perform provis sampl method analysi drawn basi present knowledg adapt account advanc scientif technolog knowledg method sampl compet author larg differ member state compet author member state posit appli provis direct short time provid suitabl period appli provis member state modifi method sampl gradual order compli provis laid annex direct time direct appli examin regularli member state applic provis measur provid direct accord opinion stand committe foodstuff adopt direct articl member state measur ensur sampl offici control level aflatoxin foodstuff carri accord method annex direct articl member state measur ensur sampl prepar method analys offici control level aflatoxin foodstuff compli criteria annex ii direct articl member state decemb bring forc law regul administr provis compli provis direct forthwith notifi commiss thereof member state adopt provis provis refer direct accompani refer time offici public procedur refer adopt member state articl direct enter forc dai public offici journal european commun direct address member state brussel juli commiss franz fischler member commiss oj page offici journal oj annex method sampl offici check control level aflatoxin foodstuff purpos scope sampl intend offici check level aflatoxin content foodstuff method aggreg sampl obtain consid repres lot complianc maximum limit laid commiss regul ec establish basi level determin laboratori sampl definit gt tabl gt gener provis personnel sampl perform authoris person member state materi sampl lot examin sampl separ accord specif provis point annex larg lot subdivid sublot sampl separ precaut sampl prepar laboratori sampl precaut avoid affect aflatoxin content advers affect analyt determin make aggreg sampl unrepres increment sampl increment sampl place distribut lot sublot departur procedur record record provid prepar aggreg sampl laboratori sampl subsampl aggreg sampl made unit suffici mix increment sampl mix aggreg sampl divid equal subsampl accord specif provis point annex mix ensur subsampl portion lot sublot replic sampl replic sampl enforc trade defenc refere purpos homogenis laboratori sampl conflict member state rule sampl packag transmiss laboratori sampl laboratori sampl clean inert contain offer adequ protect contamin damag transit precaut avoid chang composit laboratori sampl aris transport storag seal label laboratori sampl sampl offici seal place sampl identifi member state regul record sampl permit lot identifi unambigu give date place sampl addit inform assist analyst explanatori provis type lot food commod trade bulk contain individu pack sack bag retail pack sampl procedur appli form commod put market prejudic specif provis laid point annex formula guid sampl lot trade individu pack sack bag retail pack sampl frequenc sf gt num gt weight lot weight increment sampl gt den gt weight aggreg sampl weight individu pack weight kg sampl frequenc sf nth sack bag increment sampl decim figur round nearest number weight increment sampl weight increment sampl gram defin point annex case lot retail pack weight increment sampl depend weight retail pack number increment sampl lot tonn number increment sampl depend weight lot minimum maximum defin point annex figur tabl determin number increment sampl gt tabl gt specif provis gener survei sampl procedur groundnut nut dri fruit cereal gt tabl gt groundnut pistachio brazil nut dri fig cereal lot amp ge tonn sampl procedur condit sublot separ physic lot subdivid sublot tabl point take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum sublot sampl separ number increment sampl case lot tonn number increment sampl depend weight lot minimum maximum point weight aggreg sampl kg mix divid equal subsampl kg grind divis subsampl case groundnut nut dri fruit intend sort physic treatment depend avail equip homogenis kg sampl case aggreg sampl weight kg aggreg sampl divid subsampl laboratori sampl subsampl kg subsampl separ ground fine mix achiev complet homogenis accord provis laid annex ii carri method sampl commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document accept lot sublot groundnut nut dri fruit subject sort physic treatment accept aggreg sampl averag subsampl conform maximum limit reject aggreg sampl averag subsampl exce maximum limit groundnut nut dri fruit cereal intend direct human consumpt accept subsampl exce maximum limit reject subsampl exce maximum limit aggreg sampl kg accept aggreg sampl conform maximum limit reject aggreg sampl exce maximum limit nut groundnut pistachio brazil nut dri fruit fig cereal lot tonn sampl procedur product sampl procedur laid point appli take account low incid contamin product newer form packag product trade simpler sampl method appli cereal lot tonn sampl plan consist depend lot weight increment sampl gram result aggreg sampl kg figur tabl determin number increment sampl gt tabl gt accept lot sublot point milk sampl procedur sampl accord commiss decis eec februari lai method analysi test raw milk heat treat milk number increment sampl minimum weight aggreg sampl minimum kg litr accept lot sublot accept aggreg sampl conform maximum limit reject aggreg sampl exce maximum limit deriv product compound food milk product sampl procedur sampl accord commiss direct eec octob lai commun method sampl chemic analysi monitor preserv milk product number increment sampl minimum milk product equival method sampl accept lot sublot accept aggreg sampl conform maximum limit reject aggreg sampl exce maximum limit deriv product small particl weight flour fig past peanut butter homogen distribut aflatoxin contamin sampl procedur number increment sampl lot tonn number increment sampl depend lot weight tabl point annex weight increment sampl gram case lot retail pack weight increment sampl depend weight retail pack weight aggreg sampl kg suffici mix number sampl number aggreg sampl depend lot weight divis larg lot sublot defin cereal point sublot sampl separ accept lot sublot accept aggreg sampl conform maximum limit reject aggreg sampl exce maximum limit deriv product larg particl size heterogen distribut aflatoxin contamin sampl procedur accept defin point annex raw agricultur product oj oj annex ii sampl prepar criteria method analysi offici check level aflatoxin foodstuff introduct precaut daylight exclud procedur aflatoxin gradual break influenc ultra violet light distribut aflatoxin extrem homogen sampl prepar homogenis extrem care materi receiv laboratori prepar test materi calcul proport shell kernel nut limit fix aflatoxin commiss regul ec appli edibl part level aflatoxin edibl part determin shell sampl nut shell level aflatoxin directli determin edibl part homogenis nut shell take sampl prepar procedur sampl analyt procedur estim weight nut kernel aggreg sampl weight nut kernel aggreg sampl estim establish suitabl factor proport nut shell nut kernel nut proport ascertain amount kernel bulk sampl sampl prepar analysi procedur approxim nut random separ lot put aggreg sampl ratio laboratori sampl obtain weigh nut shell weigh shell kernel portion proport shell kernel establish laboratori number sampl assum futur analyt work laboratori sampl found contravent limit proport determin sampl approxim nut set treatment sampl receiv laboratori fine grind mix laboratori sampl process demonstr achiev complet homogenis subdivis sampl enforc defenc purpos replic sampl enforc trade defenc refere purpos homogenis materi conflict member state rule sampl method analysi laboratori laboratori control requir definit number commonli definit laboratori requir commonli quot precis paramet repeat reproduc gt tabl gt gener requir method analysi food control purpos compli provis point annex council direct eec specif requir specif method determin aflatoxin level foodstuff prescrib commun level laboratori select method provid select method meet criteria gt tabl gt note valu appli sum sum individu aflatoxin report respons analyt system equival detect limit method state precis valu concentr interest precis valu calcul horwitz equat rsdr logc rsdr rel standard deviat calcul result gener reproduc condit sr concentr ratio mg kg generalis precis equat found independ analys matrix sole depend concentr routin method analysi recoveri calcul analyt result report correct uncorrect recoveri manner report level recoveri report laboratori qualiti standard laboratori compli council direct eec