commiss direct ec june lai sampl method method analysi offici control level fusarium toxin foodstuff text eea relev commiss european commun regard treati establish european commun regard council direct eec decemb introduct commun method sampl analysi monitor foodstuff intend human consumpt articl thereof commiss regul ec march set maximum level contamin foodstuff maximum limit fusarium toxin foodstuff council direct eec june offici control foodstuff lai gener principl perform control foodstuff council direct eec octob subject addit measur offici control foodstuff introduc system qualiti standard laboratori entrust member state offici control foodstuff sampl plai crucial part precis determin level fusarium toxin heterogen distribut lot fix gener criteria method analysi compli order ensur control laboratori method analysi compar level perform measur provid direct accord opinion stand committe food chain anim health adopt direct articl member state ensur sampl offici control level fusarium toxin deoxynivalenol zearalenon fumonisin ht toxin foodstuff carri accord method set annex articl member state ensur sampl prepar method analys offici control level fusarium toxin deoxynivalenol zearalenon fumonisin ht toxin foodstuff compli criteria set annex ii articl member state bring forc law regul administr provis compli direct juli latest forthwith commun commiss text provis correl tabl provis direct member state adopt provis refer direct accompani refer occas offici public member state determin refer made member state commun commiss text main provis nation law adopt field cover direct articl direct enter forc twentieth dai public offici journal european union articl direct address member state brussel june commiss marko kyprian member commiss oj direct amend regul ec european parliament council oj oj regul amend regul ec page offici journal oj oj direct amend regul ec annex method sampl offici control level fusarium toxin foodstuff purpos scope sampl intend offici check level fusarium toxin content foodstuff method set annex aggreg sampl obtain consid repres lot complianc maximum limit laid annex regul ec establish basi level determin laboratori sampl definit purpos annex definit appli lot identifi quantiti food commod deliv time determin offici common characterist origin varieti type pack packer consignor mark sublot design part larg lot order appli sampl method design part sublot physic separ identifi increment sampl quantiti materi singl place lot sublot aggreg sampl combin total increment sampl lot sublot gener provis personnel sampl perform authoris person design member state materi sampl lot examin sampl separ accord point larg lot subdivid sublot sampl separ precaut sampl prepar sampl precaut avoid affect fusarium toxin content advers affect analyt determin make aggreg sampl unrepres increment sampl increment sampl place distribut lot sublot departur procedur record record prepar aggreg sampl aggreg sampl made unit increment sampl replic sampl replic sampl enforc trade defenc refer refere purpos homogenis aggreg sampl procedur conflict member state rule packag transmiss sampl sampl clean inert contain offer adequ protect contamin damag transit precaut avoid chang composit sampl aris transport storag seal label sampl sampl offici seal place sampl identifi regul member state record sampl permit lot identifi unambigu give date place sampl addit inform assist analyst specif provis type lot food commod trade bulk contain individu pack sack bag retail pack sampl procedur appli form commod put market prejudic specif provis set point formula guid sampl lot trade individu pack sack bag retail pack weight kg sampl frequenc sf nth sack bag increment sampl decim figur round nearest number weight increment sampl weight increment sampl gram defin annex case lot retail pack weight increment sampl depend weight retail pack gener survei sampl procedur cereal cereal product tabl subdivis lot sublot depend product lot weight commod lot weight tonn weight number sublot increment sampl aggreg sampl weight kg cereal cereal product tonn gt lt sublot tonn lt sampl procedur cereal cereal product lot tonn condit sublot separ physic lot subdivid sublot tabl take account weight lot exact multipl weight sublot weight sublot exce mention weight maximum sublot sampl separ number increment sampl weight aggreg sampl kg carri method sampl set point commerci consequ result damag lot packag form mean transport altern method sampl appli provid repres fulli document sampl procedur cereal cereal product lot lt tonn lot cereal cereal product tonn sampl plan increment sampl depend lot weight result aggreg sampl kg small lot tonn lower number increment sampl aggreg sampl unit increment sampl case kg figur tabl determin number increment sampl tabl number increment sampl depend weight lot cereal cereal product lot weight tonn increment sampl gt gt gt gt gt gt sampl procedur food intend infant young children sampl procedur cereal cereal product set point appli food intend infant young children number increment sampl depend weight lot minimum maximum accord tabl point small lot tonn lower number increment sampl aggreg sampl unit increment sampl case kg weight increment sampl gram case lot retail pack weight increment sampl depend weight retail pack case small lot tonn increment sampl weight unit increment sampl result aggreg sampl kg weight aggreg sampl kg suffici mix sampl retail stage sampl foodstuff retail stage accord sampl provis set point effect sampl procedur retail stage provid ensur suffici repres sampl lot accept lot sublot accept aggreg sampl conform maximum limit take account measur uncertainti correct recoveri reject aggreg sampl exce maximum limit reason doubt take account measur uncertainti correct recoveri depend lot weight tabl annex ii sampl prepar criteria method analysi offici check level fusarium toxin foodstuff precaut distribut fusarium toxin homogen sampl prepar homogenis extrem care materi receiv laboratori prepar test materi treatment sampl receiv laboratori laboratori sampl fine grind mix process demonstr achiev complet homogenis case maximum level appli dry matter dry matter content product determin part homogenis sampl procedur demonstr determin accur dry matter content subdivis sampl enforc defenc purpos replic sampl enforc trade defenc refere purpos homogenis materi procedur conflict member state rule sampl method analysi laboratori laboratori control requir definit number commonli definit laboratori requir commonli quot precis paramet repeat reproduc repeat absolut differ singl test result obtain repeat condit sampl oper apparatu laboratori short interv time expect lie specif probabl typic sr sr standard deviat calcul result gener repeat condit rsdr rel standard deviat calcul result gener repeat condit sr reproduc absolut differ singl test result obtain reproduc condit ident materi obtain oper laboratori standardis test method expect lie probabl typic sr sr standard deviat calcul result reproduc condit rsdr rel standard deviat calcul result gener reproduc condit sr gener requir method analysi food control purpos compli provis item annex direct eec specif requir perform criteria specif method determin fusarium toxin level foodstuff requir commun legisl laboratori select method provid select method meet criteria perform characterist deoxynivalenol level μg kg deoxynivalenol rsdr rsdr recoveri gt gt perform characterist zearalenon level μg kg zearalenon rsdr rsdr recoveri gt perform characterist fumonisin level μg kg fumonisin rsdr rsdr recoveri gt perform characterist ht toxin level μg kg toxin rsdr rsdr recoveri gt level μg kg ht toxin rsdr rsdr recoveri gt detect limit method state precis valu concentr interest precis valu calcul horwitz equat rsdr logc rsdr rel standard deviat calcul result gener reproduc condit sr concentr ratio mg kg generalis precis equat found independ analyt matrix sole depend concentr routin method analysi quot fit purpos quot approach case limit number fulli valid method analysi altern quot fit purpos quot approach defin singl paramet fit function evalu accept method analysi fit function uncertainti function specifi maximum level uncertainti regard fit purpos limit number method analysi fulli valid collabor trial determin ht toxin uncertainti function approach maximum accept uncertainti assess suitabl quot fit purpos quot method analysi laboratori laboratori method produc result maximum standard uncertainti maximum standard uncertainti calcul formula uf maximum standard uncertainti μg kg lod limit detect method μg kg constant numer factor depend valu set tabl concentr interest μg kg analyt method result uncertainti measur maximum standard uncertainti method consid equal suitabl meet perform characterist point tabl numer valu constant formula set point depend concentr interest μg kg gt recoveri calcul report result analyt result report correct uncorrect recoveri manner report level recoveri report analyt result correct recoveri check complianc annex point analyt result report analyt result expand measur uncertainti expand uncertainti coverag factor level confid approxim laboratori qualiti standard laboratori compli council direct eec