commiss regul ec decemb lai detail rule applic council regul ec intervent market butter cream commiss european commun regard treati establish european commun regard council regul ec common organis market milk milk product articl thereof regul ec replac council regul eec amend regul ec inter alia council regul eec amend regul eec intervent arrang butter skim milk powder view arrang light experi gain amend simplifi detail rule govern intervent market butter cream interest clariti recast specif regul govern aspect intervent commiss regul eec amend regul ec eec amend regul ec eec amend regul ec ec amend regul ec undertaken articl regul ec lai criteria intervent agenc bui butter invit tender bui suspend firstli case bui open suspend member state concern fix repres period level market price butter relat intervent price record end quot market price butter quot defin arrang set record price nation level practic reason belgo luxembourg econom union consid singl member state intervent agenc bui butter meet requir laid articl regul ec condit qualiti present defin method analysi detail rule govern qualiti control situat requir provis made check radioact butter maximum level establish commun legisl member state authoris system check subject condit practic reason period butter offer intervent produc extens interv invit tender longer dai ensur intervent arrang function smoothli condit approv manufactur undertak verif complianc therewith ensur arrang effect provis made action condit compli butter bought intervent agenc belong member state territori produc intervent agenc bui case verifi condit relat qualiti present compli regul ec stipul bui carri tender procedur ensur interest parti commun treat equal invit tender advertis offici journal european commun detail tender minimum quantiti deadlin submiss maximum bui price defin ensur complianc requir qualiti present butter time tender submit entri storag tender requir submit written undertak effect tender tender accompani secur order guarante tender maintain close date submiss tender butter deliv time limit laid guarante qualiti butter term bui mean check stage storag failur compli requir impos addit burden commun budget provis made standard butter back oper oblig bear storag cost incur member state oblig view proper manag stock storag stipul maximum distanc place storag cost born distanc exceed requir stock access batch identifi butter storag insur risk order ensur uniform frequenc level check natur number inspect storag premis perform nation author proper manag intervent stock requir butter resold outlet ensur equal access butter sale interest parti bui order destabilis market sell price fix regard market situat condit sale entail lodg perform bond laid take butter time limit payment order monitor situat stock member state inform commiss quantiti butter sold articl regul ec aid grant privat storag butter cream ensur arrang monitor properli provis made contract set specif storag condit reason detail rule laid document account frequenc check inspect procedur respect requir laid articl facilit check presenc product store privat storag contract provis remov storag lot member state authoris remov smaller quantiti ensur privat storag scheme properli manag fix annual basi storag period amount aid date entri storag date storer remov storag part quantiti compris contract date storag period aid amount chang account market situat case aid cream order account product practic reason amount aid fix butter equival fat content justifi requir fat content check systemat end storer requir undertak compli minimum fat content fix advanc entir storag period experi shown case desir eas administr burden provid check sampl imposs verifi fat content cream freez abovement undertak compli aid paid lot storag recent satisfactori check subparagraph articl regul ec amount aid increas market warrant condit determin adjust scope defin regul ec fix intervent price juli interest clariti intervent price applic date entri forc regul june measur provid regul accord opinion manag committe milk milk product adopt regul chapter scope articl regul lai detail rule appli intervent measur milk milk product sector provid articl regul ec purpos regul belgo luxembourg econom union consid singl member state chapter ii public storag section condit bui butter articl observ member state week success market price lower intervent price commiss commenc bui tender procedur provid articl regul ec member state concern accord procedur laid articl regul observ member state week success market price equal higher intervent price commiss suspend bui tender procedur provid articl regul ec member state concern accord procedur laid articl regul articl intervent agenc bui butter meet provis contain subparagraph articl regul ec articl regul articl compet author check qualiti butter analyt method set annex ii iii basi sampl accord rule set annex iv member state commiss agre set system check supervis respect qualiti requir case approv undertak level radioact butter exce maximum level permit applic commun rule level radioact contamin product monitor situat requir requisit period durat scope check determin accord procedur laid articl regul ec butter made dai preced close date submiss tender refer articl interv consecut invit tender longer dai butter made period minimum quantiti butter offer tonn member state requir butter offer full tonn butter packag deliv block kilogram net butter pack strong materi ensur protect transport storag remov storag packag show particular code approv number identifi factori member state product date product date entri storag product batch number packag number packag number replac pallet number mark pallet word quot sweet cream quot aqueou phase butter ph nation qualiti class refer annex requir member state product member state waiv oblig show date entri storag packag provid store manag undertak regist particular refer subparagraph record date entri storag articl undertak refer articl regul ec approv approv accord articl council direct eec technic equip undertak perman record form determin compet agenc member state list origin raw materi quantiti butter obtain packag identif exit date product batch intend public intervent agre submit product butter specif offici inspect applic meet requir nation qualiti class refer annex undertak inform compet agenc respons inspect work dai advanc intent produc butter public intervent member state set shorter time limit ensur complianc regul compet agenc carri unannounc spot inspect basi intervent butter product schedul undertak concern carri inspect period dai product intervent inspect month examin record refer paragraph inspect month verifi complianc condit approv refer paragraph approv withdrawn precondit laid paragraph longer satisfi approv regrant request enterpris concern period month inspect case forc majeur enterpris found compli undertak refer paragraph approv suspend period month depend serious irregular member state impos suspens found irregular commit deliber result neglig minor import regard effect inspect provid paragraph report drawn inspect carri pursuant paragraph date inspect durat oper carri report sign inspector respons member state inform commiss measur regard inspect provid paragraph month adopt articl butter offer intervent member state produc bui subject present certif suppli dai close date submiss tender compet agenc member state product certif inform refer articl applic confirm butter produc directli exclus pasteuris cream mean indent articl regul ec approv undertak commun member state product perform check refer articl certif result check confirm product concern butter mean subparagraph articl regul ec case packag refer articl seal mean number label issu compet agenc member state product number enter certif refer paragraph section price record articl market price butter refer articl regul ec price factori payment dai exclus nation tax charg fresh butter meet condit set subparagraph articl regul ec packag block kilogram net factori price rais flat rate amount eur kilogram account transport cost deliv butter cold storag plant articl market price nation level record week price board repres market weekli record price relat price provid articl record preced week price express euro round decim place kilogram member state determin membership price board ensur buyer seller engag transact involv larg quantiti butter equal repres case system record price repres market provis need check data price record base case transact relat butter qualiti refer paragraph articl insuffici volum deem repres criteria establish ratio price butter transact butter refer articl member state provid commiss descript arrang set accord subparagraph noon brussel time wednesdai member state inform commiss price record accord paragraph thursdai commiss record level market price member state comparison intervent price section tender procedur articl commiss note condit refer articl fulfil member state intervent agenc concern bui butter accord section notic invit tender publish offici journal european commun articl close date submiss tender individu invit tender fall fourth tuesdai month noon brussel time tuesdai august fourth tuesdai decemb tuesdai public holidai close date preced work dai noon brussel time articl interest parti particip tender procedur announc intervent agenc member state submit written tender issuanc receipt written mean telecommun proof receipt tender address tender quantiti offer minimum fat content propos price kilogram butter exclus nation tax charg deliv load bai cold store express euro decim place place butter held tender valid relat quantiti butter meet requir articl accompani written undertak tender compli articl proof furnish tender lodg secur eur kg invit tender concern member state tender submit close date submiss tender undertak provid paragraph forward initi intervent agenc deem tacitli renew subsequ tender explicitli cancel tender intervent agenc provid origin tender stipul tender intend avail provis subsequ tender refer provis articl date origin tender intervent agenc record dai tender receiv quantiti involv respect date manufactur place butter offer store tender withdrawn close date refer articl submiss tender relat invit tender concern articl mainten tender close date submiss tender deliveri butter depot design intervent agenc time limit laid articl constitut primari requir mean articl commiss regul eec articl member state inform commiss quantiti price offer tender brussel time dai close date refer articl light tender receiv invit tender commiss fix maximum bui price refer intervent price applic accord procedur laid articl regul ec decis proce invit tender articl tender refus price propos higher maximum price refer articl appli tender procedur concern right oblig result tender procedur transfer articl tender inform immedi intervent agenc outcom particip tender procedur tender unsuccess secur refer articl releas immedi intervent agenc immedi issu success tender date number deliveri order indic quantiti deliv final date deliveri butter cold storag depot deliv dai close date submiss tender success tender deliv butter load bai cold store deliveri consign cost incur unload butter load bai cold store born success tender secur releas success tender deliv quantiti deliveri order time limit laid case forc majeur success tender fail deliv butter time limit laid secur provid articl forfeit proport quantiti deliv bui cancel respect remain quantiti articl intervent agenc pai success tender price tender quantiti butter dai afrer take provid complianc provis articl confirm dai take dai butter enter cold store design intervent agenc earlier dai deliveri order refer articl issu articl butter put trial storag period period fix dai start dai take tender seller undertak inspect entri store design intervent agenc show butter meet provis articl end trial storageperiod minimum organolept qualiti butter prove set annex back butter question pai storag cost butter concern dai date remov storag storag cost paid cost reimburs intervent agenc account guarante section european agricultur guidanc guarante fund eaggf accord articl commiss regul eec amount credit account european agricultur guidanc guarante fund eaggf guarante section section entri remov storag articl member state lai technic standard provid storag temperatur lower cold store refer subparagraph articl regul ec measur need ensur butter properli conserv relev risk cover insur form contractu oblig storer comprehens coverag liabil born intervent agenc member state act insur intervent agenc requir butter deliv load bai cold store storag pallet creat easili identifi readili access lot compet agenc respons check perform unannounc check presenc butter store accord articl commiss regul ec articl intervent agenc choos cold store nearest place butter store provid choic cold store result addit storag cost choos store situat distanc refer paragraph choos cold store situat distanc result expenditur inclus storag transport cost lower case intervent agenc notifi commiss choic forthwith maximum distanc refer subparagraph articl regul ec kilometr distanc addit transport cost born intervent agenc eur tonn kilometr intervent agenc bui butter member state territori offer butter store account calcul maximum distanc refer subparagraph distanc store vendor border member state purchas intervent agenc addit charg refer paragraph born intervent agenc temperatur butter exce arriv cold store articl time remov store intervent agenc case deliveri cold store make butter pallet store loadingbai load mean transport lorri railwai wagon cost involv born intervent agenc stowag depalletis cost born purchas butter section sale butter articl intervent agenc member state sell interest parti butter hold enter storag juli articl butter sold storag depot price equal intervent price fix articl regul ec appli dai sale contract conclud eur kg sold quantiti tonn quantiti remain storag depot tonn sale relat smaller quantiti intervent agenc sell butter secur equal eur kg lodg conclus contract sale order ensur primari requir mean articl regul eec fulfil take butter time limit laid subparagraph articl regul intervent agenc sell butter date storag start oldest total quantiti case quantiti store store design purchas articl purchas deliveri butter month date sale contract conclud deliveri instal tonn quantiti remain storag depot tonn smaller quantiti deliv take deliveri quantiti butter purchas pai intervent agenc price quantiti deliv event forc majeur sale contract termin respect quantiti purchas deliveri period paragraph secur provid articl forfeit respect quantiti contract sale termin accord paragraph releas immedi respect quantiti deliveri prescrib period event forc majeur intervent agenc action consid regard circumst invok articl member state inform commiss tuesdai week quantiti butter preced week subject sale contract chapter iii privat storag butter cream section contract storag condit articl purpos chapter quot storag lot quot mean quantiti weigh tonn homogen composit qualiti origin singl factori storag singl warehous singl dai quot dai commenc contractu storag quot mean dai entri store quot dai contractu storag quot mean dai preced remov storag articl contract relat privat storag butter cream refer fourth subparagraph articl regul ec conclud intervent agenc member state territori butter cream store natur legal person hereinaft call quot contractor quot articl privat storag contract conclud butter cream refer subparagraph articl regul ec butter produc undertak approv accord articl regul dai preced dai commenc contractu storag correspond nation qualiti class member state product refer annex radioact level exce maximum permit level refer articl storag contract conclud butter cream respect applic direct consumpt aid made commun provis arrang refer articl council regul eec subsequ place arrang regard end contractu storag period articl storag contract conclud write storag lot includ provis quantiti butter cream contract appli amount aid prejudic articl date relat execut contract prejudic subparagraph articl regul ec ident cold store control measur refer articl inform refer paragraph articl subject specif drawn intervent agenc member state storag storag contract refer specif specif provid packag butter show particular encod number identifi factori member state product date product date entri storag number manufactur batch word quot salt quot case butter refer indent subparagraph articl regul ec nation qualiti class refer annex net weight member state waiv oblig date entri store packag provid store manag undertak regist particular refer subparagraph enter date entri store articl entri store place march august year remov store place august year storag remov store storag lot compet agenc authoris smaller quantiti circumst refer articl seal quantiti remov store articl applic conclud contract intervent agenc relat lot butter cream fulli storag applic reach intervent agenc dai date entri store intervent agenc regist date receipt applic reach intervent agenc work dai deadlin storag contract conclud aid reduc storag contract conclud dai date registr applic articl butter store member state member state product conclus storag contract refer articl subject present certif suppli compet agenc member state product dai date butter entri storag certif inform articl confirm product concern butter mean subparagraph articl regul ec case refer paragraph storag contract conclud dai date registr applic section check articl member state ensur condit entitl payment aid fulfil contractor request member state authoris person respons storag depot make compet agenc respons inspect document permit verif particular product privat storag approv number identifi factori member state product date product date entri storag storag lot number presenc store address store date remov storag contractor applic person respons store stock record store contract cover storag lot number product privat storag date entri remov storag quantiti butter cream storag lot locat product store product store easili identifi easili access identifi individu contract articl entri storag compet agenc conduct check period begin date entri store end dai date registr applic conclus contract refer articl ensur product store elig aid check made repres sampl quantiti storag ensur suffici inter alia weight identif natur product storag lot entireti physic conform applic conclus contract compet agenc seal product contract storag lot smaller quantiti time check provid paragraph make unannounc check sampl ensur product present store sampl concern repres correspond total quantiti contract privat storag aid measur end contractu storag period compet agenc sampl verifi weight identif end contractor inform compet agenc work dai end maximum contractu storag period dai product remov dai period start remov oper indic storag lot involv butter storag expiri maximum contractu storag period check refer subparagraph made butter remov storag end contractor inform compet agenc work dai start remov oper case provid subparagraph member state accept shorter timelimit work dai report drawn check carri pursuant paragraph date check durat oper carri report sign inspector respons countersign contractor case person respons store includ payment dossier event irregular affect quantiti product check check extend larger sampl determin compet agenc member state notifi case commiss week section storag aid articl aid privat storag provid subparagraph articl regul ec grant contractu storag period dai contractor fail compli time limit refer articl aid reduc paid respect period contractor suppli satisfactori proof compet agenc butter cream remain contractu storag prejudic articl commiss determin year accord procedur laid articl regul ec amount aid refer subparagraph articl regul privat storag contract commenc year question aid paid applic contractor end contractu storag period dai receipt applic provid check refer articl carri condit entitl aid met administr enquiri entitl aid payment made entitl recognis dai contractu storag singl advanc payment aid made contractor request provid lodg secur equal advanc payment advanc calcul basi storag period dai secur releas balanc aid refer paragraph paid articl end dai contractu storag deterior qualiti butter cream greater normal store contractor authoris storag lot replac defect quantiti expens equal quantiti butter cream subparagraph articl regul ec check storag remov reveal defect quantiti aid paid quantiti addit remaind storag lot elig aid tonn rule appli part lot remov august expiri minimum storag period purpos calcul aid case refer subparagraph paragraph dai contractu storag dai commenc contractu storag articl aid storag cream grant pasteuris cream fat content purpos calcul aid quantiti cream convert butter equival refer butter fat content multipli fat content cream fat content paragraph check laboratori approv compet agenc cream frozen articl member state permit contractor undertak voluntarili storag lot contract conclud current year observ singl minimum fat content fix advanc limit articl paragraph appli aid grant basi minimum fat content fix advanc case member state check fat content accord articl random sampl frequent unannounc visit check reveal fat content lower minimum content fix advanc aid paid storag lot store satisfactori check paragraph longer appli contractor concern rest contractu storag period fat content found lower minimum content fix advanc aid paid basi fat content found minu articl market situat requir amount aid period entri remov storag maximum length storag alter year respect contract conclud maximum bui price fix invit tender accord articl express euro countri particip singl currenc nation currenc appli dai commenc contractu storag higher appli dai contractu storag aid determin accord articl increas amount equal reduct maximum bui price excess price appli dai commenc contractu storag price lower price appli dai contractu storag aid determin accord articl reduc amount equal increas maximum bui price excess price appli dai commenc contractu storag reduct aid exce total amount aid aid adjust refer paragraph appli contractu storag period maximum bui price fix accord articl dai contractu storag bui commenc member state maximum bui price fix dai immedi preced start contractu storag period maximum bui price deem appli dai contractu storag equal intervent price forc chapter iv transit final provis articl regul eec no ec repeal regul ec continu appli privat storag contract conclud januari refer repeal regul constru refer regul articl intervent price butter appli januari june fix council regul ec articl regul enter forc januari regul bind entireti directli applic member state brussel decemb commiss franz fischler member commiss oj oj oj oj oj oj oj oj oj oj oj oj oj oj oj oj oj oj oj annex composit requir qualiti characterist analyt method gt tabl gt annex ii refer method detect foreign fat milk fat ga chromatograph analysi triglycerid revis scope field applic standard lai method detect foreign fat veget fat anim fat beef tallow lard milk fat milk product ga chromatograph analysi triglycerid defin triglycerid formula veget anim fat qualit quantit detect pure milk fat irrespect feed lactat condit note butyr acid occur exclus milk fat enabl quantit estim low amount milk fat veget fat made qualit quantit inform provid rang addit weight foreign fat pure milk fat larg variat rang approxim weight note quantit result practic obtain trigylcerid analys sterol content veget fat function product treatment condit definit foreign fat milk fat foreign fat defin standard veget anim fat milk fat principl method extract milk fat stock solut prepar solut triglycerid total carbon number determin ga chromatograph pack column insert weight fat molecul size number triglycerid formula foreign fat qualit detect quantit determin note observ evalu capillari ga chromatographi guarante compar result achiev reagent analysi grade chemic carrier ga nitrogen puriti degre amp gt standard triglycerid satur cholesterol standard standard milk fat section methanol water free hexan heptan toluen dimethylchlorosilan solut ml dimethylchlorosilan dissolv ml toluen combust ga hydrogen synthet air stationari phase ov μm mesh ga chromq cocoa butter solut instrument normal laboratori apparatu high temperatur ga chromatograph suit temperatur equip flame ioniz detector fid constant mass flow control carrier ga combust ga ml min ml min synthet air note high temperatur occur triglycerid analys glass insert fid injector system frequent clean ga chromatograph msut equip septa withstand high temperatur frequent exhibit gener low degre quot bleed quot note suit chromblu tm septa chrompack septa exchang regular interv roughli inject resolut deterior figur chromatographi column shape glass column insid diamet mm mm length silan section dimethylchlorosilan order deactiv glass surfac note suit longer mm length pack column slightli reproduc result achiev hand stationari phase exhibit occasion fractur oper lead turn wors quantit result fid flame easili extinguis result requir extrem high carrier ga flow ml min arrang fill column figur figur fill column gt pic file quot en ep quot gt plastic column screw end cap provid mark requir quantiti stationari phase fill fine siev mesh size approxim μm screw cap suit seal glass column figur deactiv silan glass wool vibrat uniform distribut stationari phase fill ml extrelut column silica gel column altern extract obtain milk fat graphit seal mm quot mm bore devic silan glass surfac column section woulff bottl water suction pump water bath adjust dry cabinet adjust microlitr pipett ml graduat pipett dose ml methanol ml round bottom flask erlenmey flask nomin volum ml funnel fine pore filter rotari evapor ampoul nomin volum ml sealabl aluminium cap septum interior inject syring plunger syring reach tip needl note syring reproduct result obtain oder avoid deterior septum tip needl check regular interv stereomicroscop procedur prepar column silan connect woulff bottl shown figur water suction pump tube dip solut section close stopcock column fill subsequ tube remov figur arrang silanis gt pic file quot en ep quot gt column fix stand complet fill dimethyldichlorosilan solut mean pipett min woulff bottl replac filter flask column empti connect water suction pump figur fill column success rins ml toluen ml methanol empti column dri dry cabinet approxim minut figur arrang rins gt pic file quot en ep quot gt fill column arrang repres figur stationari phase fill plastic column mark lower end glass column fill seal approxim cm long plug glass wool silan press steel rod end column close siev section column fill pressur bar stationari phase obtain uniform continu firm pack vibrat move glass column fill fill solid plug silan glass wool press end pack column protrud end cut plug press column millimetr spatula prepar sampl sampl prepar method isol milk fat butter butter melt suitabl vessel water bath section ml erlenmey flask funnel insert filter section heat dry cabinet fat layer molten butter sampl filter preheat devic milk fat phospholipid free extract fat fraction röse gottlieb method extract idf standard milk fat phospholipid cholesterol peak obtain increas approxim triglycerid spectrum standard cholesterol influenc neglig extent extract milk silica gel column ml milk sampl temper appli ml extrelut column microlitr pipett section allow distribut uniformli silica gel approxim minut denatur protein lipid complex ml methanol ad pipett subsequ sampl extract ml hexan hexan slowli ad small amount solvent drain collect ml round bottom flask dri constant weight extract led column drain empti eluat solvent distil rotatori evapor water bath temperatur flask dri fat yield determin weigh note fat extract gerber weibul berntrop schmid bondzynski ratzlaff isol milk fat deterg bdi method suit triglycerid analysi method larg quantiti partial glycerid phospholipid pass fat phase prepar sampl solut ga chromatographi solut fat heptan obtain section prepar sampl solut amount sampl materi obtain section weigh dissolv amount heptan sampl prepar section amount heptan ad sampl materi flask calcul basi weigh remain dissolv approxim ml sampl solut fill ampul section chromatograph triglycerid determin high temperatur elut long chain triglycerid increas baselin occur easili column adequ condit begin rise baselin high temperatur avoid complet combin column baselin subtract compens mode oper singl column glass insert injector detector graphit seal section baselin correct avoid baselin rise method combin column pack column compens mode baselin correct ga chromatograph applic run ga chromatograph inject fat solut subsequ subtract store baselin rise baselin avoid baselin correct integr softwar applic run integr system inject fat solut subsequ subtract store baselin rise baselin avoid baselin correct adequ condit adequ initi condit column approxim inject milk fat solut baselin rise high temperatur frequent low baselin correct inject techniqu avoid discrimin effect quot hot inject quot techniqu appli achiev quantit result high boil triglycerid compon fat solut drawn syring cold needl syring warm prior inject approxim second injector head τhen syring content rapidli inject note inject techniqu risk fraction phenomena insid syring inject block reduc quot column quot direct inject upper extend heat part column appli fragment septum accumul contamin easili elimin techniqu regularli chang injector insert dismount column bend tip needl caus touch bottom sampl beaker visibl ey alsolut avoid order damag septum figur triglycerid chromatogram milk fat sampl gt pic file quot en ep quot gt condit pack column step top column connect detector avoid contamin column fill section condit min ml min flow heat min ml min hold inject μl cocoa butter solut section respect temperatur program inject μm milk fat solut dai section note cocoa butter consist exclus high boil triglycerid inject cocoa butter serv purpos special condit long chain rang high boil triglycerid partli respons factor approxim occur repeat inject milk fat solut reduct initi high respons factor expect triglycerid low acyl number factor approxim pair column fill section prepar condit pair check milk fat analysi routin test pair quantit result respons factor respons factor amp gt column calibr calibr respons factor triglycerid cholesterol milk fat standard fat determin standard triglycerid satur triglycerid cholesterol addition intermedi respons factor found mathemat interpol standard fat calibr perform dai ident result obtain reproduc quantit result achiev triglycerid analysi sampl standard milk fat stock life month storag temperatur maxim standard temperatur programm carrier ga condit triglycerid analysi temperatur programm initi column temperatur hold minut program min hold final temperatur minut detector injector temperatur note detector injector oven temperatur initi temperatur maintain constant level overnight weekend holidai carrier ga nitrogen flow rate ml min note cm column flow ml min carrier ga flow constantli maintain overnight weekend holidai exact carrier ga flow adjust manner independ column length elut durat analysi minut inject volum μl note syring rins time pure heptan inject fid condit section note flame ioniz detector ignit begin work dai integr evalu control measur condit triglycerid odd acyl number combin preced number triglycerid reproduc low content account remain triglycerid peak area chromatogram includ cholesterol peak multipli respect respons factor standard fat calibr altogeth normal free cholesterol triglycerid evalu result weight evalu chromatogram peak integr baselin plot reintegr optim integr paramet figur demonstr exampl triglycerid chromatogram figur show chromatogram evalu whilst figur repres sporad error rang baselin run incorrectli compar figur typic error detect high degre certainti avoid integr baselin plot figur easi evalu triglycerid chromatogram milk fat baselin drawn gt pic file quot en ep quot gt figur wrongli integr chromatogram milk fat gt pic file quot en ep quot gt control measur condit tabl show valu standard deviat sd typic winter milk fat triglycerid analys fat tabl triglycerid composit milk fat valu sd analys gt tabl gt sd deviat greater extent compar valu tabl chromatogram toler septa ga flow check small compon septum form deposit glass wool entranc column column unsuit result ag temperatur influenc figur qualit foreign fat detect detect foreign fat triglycerid formula tabl limit tabl develop valu pure milk fat fluctuat limit transgress presenc foreign fat assum sensit formula detect lard addit gt tabl gt note milk fat sampl confid rang establish pure milk fat sampl standard deviat valu sd start triglycerid composit unknown fat sampl formula comput verifi simpl manner sum triglycerid content state factor fall rang foreign fat addit detect foreign fat tabl show triglycerid formula detect foreign fat soybean oil sunflow oil oliv oil rape seed oil linse oil wheat germ oil maiz germ oil cotton seed oil hydrogen fish oil veget fat coconut palm kernel fat palm oil beef tallow common formula triglycerid composit foreign fat subject fluctuat experiment measur foreign fat triglycerid data type foreign fat type favour limit consid tabl quot total formula quot similarli good result obtain foreign fat gt refer graphic gt calcul detect foreign fat combin milk fat shown formula lard tabl limit foreign fat low fat coconut fat palm oil palm kernel fat detect limit formula detect extrem high amount ad milk fat appli formula tabl tabl triglycerid formula detect foreign fat milk fat indic standard deviat sd formula soybean sunflow oliv rape seed linse wheat germ maiz germ cotton seed fish oil gt refer graphic gt formula coconut palm kernel fat gt refer graphic gt formula palm oil beef tallow gt refer graphic gt formula lard gt refer graphic gt check unknown fat sampl formula tabl total formula sampl mixtur milk fat foreign fat combin foreign fat insert triglycerid fat sampl analys obtain fall rang tabl formula sampl modifi milk fat detect foreign fat milk fat mean formula tabl conclus drawn type foreign fat admixtur tabl limit milk fat gt tabl gt tabl detect limit foreign fat confid column show minim detect limit milk fat formula tabl column detect limit total formula limit higher formula detect bit higher amount foreign fat formula combin foreign fat detect rang variat triglycerid foreign fat type consider influenc detect limit tabl limit detect addit foreign fat milk fat gt tabl gt quantit foreign fat determin order obtain quantit inform foreign fat concentr milk fat sampl formula gt tabl gt quantiti unknown foreign fat foreign fat mixtur unknown milk fat result addit unknown foreign fat insert triglycerid foreign fat milk fat mixtur total triglycerid formula unknown foreign fat ad milk fat foreign fat total formula chosen sf obtain insert triglycerid data pure foreign fat formula calcul sf good quantit result foreign fat addit obtain palm oil beef tallow formula tabl sf foreign fat type sf valu insert formula respect foreign fat formula tabl chosen tabl sf valu foreign fat gt tabl gt rang applic detect method method appli bulk milk base repres milk fat sampl highli specif detect repres number milk fat formula deriv countri suit possibl detect obtain countri formula set repres number milk fat case complex comput programm requir triglycerid combin tabl appli factor redetermin method squar appli rang shown tabl formula feed condit instanc underfeed feed cow feed yeast ca soap gener applic case extrem feed condit high uptak pure feed oil high administr ca soap combin feed fat formula partli modifi milk fat note fraction milk fat gener recogn unmodifi milk fat modif assum limit exceed fraction milk fat unusu milk fat composit case hard fraction obtain fraction physic method high temperatur approxim low yield percent fraction overcrit formula modif milk fat fraction detect procedur differenti scan calorimetri accuraci method determin milk fat basi formula tabl rang tabl repeat differ valu determin carri shortest feasibl time interv oper procedur ident sampl materi condit person instrument devic laboratori tabl repeat limit formula gt tabl gt reproduc differ valu determin carri oper laboratori procedur ident sampl materi condit person instrument time tabl reproduc limit formula gt tabl gt critic differ repeat reproduc limit critic differ rang tabl calcul duplic analys respect valu tabl tabl critic differ triglycerid formula gt tabl gt accept result calibr round decim calcul triglycerid content cholesterol normal result duplic analysi check repeat absolut differ result triglycerid formula transgress repeat limit tabl repeat requir met control optim ga chromatograph condit qualiti column guarante repetit run differ maximum minimum valu triglycerid formula transgress rang run literatur repeat limit formula tabl quot standard gt tabl gt refer commiss european commun detect foreign fat milk fat mean ga chromatograph triglycerid analysi doc vi en vi commiss european commun control butter fat puriti sampl feed period eec countri doc vi commiss european commun consider result fourth sixth eec collabor trial determin triglycerid milk fat doc vi vi vi vi vi vi timm detect quantif milk fat mixtur milk milk fat dairi research precht hein nachwei von modifiziertem milchfett mit der triglyceridanalys fremdfettnachwei im milchfett mit hilf von triglyceridkombinationen luf stock brandl zum nachwei von fremdfett milchfett über die trigylceridanalys österr milchwirtsch wissensch beilag precht bestimmung von pflanzlichen fetten oder tierischen depotfetten milchfett kieler milchwirtsch forschungsb precht schnell extrakt von milchfett kieler milchwirtsch forschungsb precht schnell gaschromatographisch triglyceridanalys von milchfett kieler milchwirtsch forschungsb precht control milk fat puriti ga chromatograph triglycerid analysi kieler milchwirtsch forschungsb precht detect adulter milk fat fatti acid triglycerid analysi fat sci technol precht detect foreign fat milk fat qualit detect triacylglycerol formula ii quantit evalu foreign fat mixtur lebensm unter forsch precht ga chromatographi triacylglycerol lipid pack column crc handbook chromatographi analysi lipid ed mukherje weber sherma crc press boca raton precht molkentin quantit triglycerid analysi short capillari column chrompack new molkentin precht comparison pack capillari column quantit ga chromatographi triglycerid milk fat chromatographia stang angewandt statistik erster teil eindimensional problem springer verlag berlin suit method precht molkentin quantit triglycerid analysi short capillari column chrompack new suitabl product commerci trade name extrelut ga chromq chrompack exampl suit product specialis trade inform serv purpos easi handl standard user repres request product indic grain transfer si unit μm bs quot british standard specif test siev quot footnot page annex iii sensori evalu butter scope purpos procedur sensori evalu butter provid uniform method applic member state definit sensori evalu assess mean examin attribut product sens organ panel mean group select assessor work assess intercommun influenc score mean sensori evalu panel numer scale nomenclatur defect grade mean qualiti classif perform basi score control document document record individu score attribut final grade product document record chemic composit test room precaut order assessor test room influenc extern factor test room free foreign odour easi clean wall light colour test room light properti product score affect room equip temperatur control select assessor assessor familiar butter product compet carri sensori grade compet assess regular basi year compet author requir panel number assessor panel uneven minimum number major employe compet author author person emploi dairi industri assess attribut sensori evalu carri relat attribut appear consist flavour appear involv featur colour visibl puriti mould growth water dispers water dispers test idf standard consist involv featur firm spreadabl physcial method appli evalu butter consist commiss envisag futur harmon method flavour involv featur tast odour signific deviat recommend temperatur prevent reliabl evalu consist flavour temperatur paramount import attribut sensori evalu separ score tabl desir assessor score start assess refer sampl appear consist flavour order achiev uniform score accept gt tabl gt requir score obtain descript defect score assessor attribut record control document product accept reject basi major decis case differ individu score attribut wider adjac point occur frequent sampl compet panel check panel leader supervis panel leader offici employe compet author member panel gener respons entir procedur record individu score attribut control document certifi product accept reject sampl prepar sampl desir ident sampl conceal assess bia avoid organ panel leader prior evalu presenc panel member sensori evalu carri cold store sampl butter trier sensori evalu carri locat cold store sampl evalu butter temperatur larg deviat avoid cost nomenclatur refer append tabl tabl butter score gt tabl gt gt tabl gt gt tabl gt tabl tabl butter defect appear loos free moistur uniform colour streaki mottl marbl speckl oil separ overcolour weak open textur granular foreign matter mouldi undissolv salt ii consist short brittl crumbl pasti doughi greasi sticki hard soft iii flavour amp aroma flavour unclean foreign flavour stale cheesi lactic chees flavour acid yeasti cook flavour scorch flavour mouldi flavour rancid oili fishi tallowi oxid flavour metal flavour feed flavour coars bitter oversalt musti flat putrid malti chemic flavour design seldom defect accur annex iv sampl chemic microbiolog analysi sensori evalu chemic microbiolog analysi gt tabl gt sampl microbiolog analysi carri asept sampl combin sampl analysi mix sampl randomli part offer quantiti test time entri cold store design intervent agenc prepar composit butter sampl chemic analysi clean dry butter trier similar suitabl instrument extract core butter place sampl contain composit sampl seal forward laboratori analysi laboratori composit sampl warm origin unopen contain shaken frequent homogen fluid emuls free unsoften piec obtain contain half third full sampl year produc offer butter intervent analys milk fat sampl tracer sensori evalu gt tabl gt sampl randomli part offer quantiti dai butter grade sampl assess individu accord annex iii resampl evalu allow guidelin sampl show defect chemic microbiolog analysi individu sampl analys sampl show singl defect sampl sampl show singl defect sampl allow sampl show defect sampl side sampl show defect check paramet question sampl meet specif quantiti butter origin sampl side sampl show defect reject quantiti offer quantiti reject sampl show defect gt pic file quot en ep quot gt composit sampl analys found show defect respect paramet quantiti repres composit sampl concern reject quantiti offer quantiti repres composit sampl determin subdivid quantiti offer sampl randomli part thereof sensori evalu sampl fail sensori evalu quantiti butter neighbour sampl side sampl fail reject quantiti offer sampl show sensori defect chemic microbiolog defect quantiti reject annex nation qualiti class quot beurr marqu de contrôl quot belgian butter quot smør første kvalitet quot danish butter quot markenbutt quot german butter quot pasteurisé quot french butter quot irish creameri butter quot irish butter quot produc exclus cream subject centrifug pasteur treatment quot italian butter quot marqu rose quot quot beurr de premièr qualité quot luxembourg butter quot extra kwaliteit quot dutch butter quot extra select quot great britain butter quot premium quot northern ireland butter quot produc exclus cream subject centrifug pasteur treatment quot greek butter quot produc exclus pasteur cow milk cream quot spanish butter quot produc exclus pasteur cow milk cream quot portugues butter quot teebutt quot austrian butter quot perinteinen meijerivoi traditionellt mejerismör quot finnish butter quot svenkst smör quot swedish butter