The method 4 wherein said {HEAD ~ cooling rate} in {TAIL ~ step} is about 0.2° C. per minute or less 
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The method 4 wherein said { HEAD ~ cooling rate } in { TAIL ~ step } is about 0.2 ° C. per minute or less
OTH OTH OTH OTH OTH HEAD HEAD HEAD HEAD HEAD HEAD REL TAIL TAIL TAIL TAIL TAIL OTH OTH OTH OTH OTH OTH OTH OTH OTH