Reaction is effected between an aryliodonium tosylate and {HEAD ~ an active hydrogen aliphatic organic compound}, such as {TAIL ~ dimedone}, to produce an intermediate arylalkyliodonium tosylate salt which is thereafter reacted with a polyfluoro metal or metalloid salt of an alkali or alkaline earth metal to produce the desired arylalkyliodonium polyfluoro metal or metalloid salt, such as dimedonylphenyliodonium hexafluoroarsenate 
such as
Reaction is effected between an aryliodonium tosylate and { HEAD ~ an active hydrogen aliphatic organic compound } , such as { TAIL ~ dimedone } , to produce an intermediate arylalkyliodonium tosylate salt which is thereafter reacted with a polyfluoro metal or metalloid salt of an alkali or alkaline earth metal to produce the desired arylalkyliodonium polyfluoro metal or metalloid salt , such as dimedonylphenyliodonium hexafluoroarsenate
OTH OTH OTH OTH OTH OTH OTH OTH HEAD HEAD HEAD HEAD HEAD HEAD HEAD HEAD HEAD HEAD OTH REL REL TAIL TAIL TAIL TAIL TAIL OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH OTH