Reaction is effected between an aryliodonium tosylate and an active hydrogen aliphatic organic compound, such as {HEAD ~ dimedone}, to produce an intermediate arylalkyliodonium tosylate salt which is thereafter reacted with {TAIL ~ a polyfluoro metal or metalloid salt} of an alkali or alkaline earth metal to produce the desired arylalkyliodonium polyfluoro metal or metalloid salt, such as dimedonylphenyliodonium hexafluoroarsenate 
Reaction is effected between an aryliodonium tosylate and an active hydrogen aliphatic organic compound , such as { HEAD ~ dimedone } , to produce an intermediate arylalkyliodonium tosylate salt which is thereafter reacted with { TAIL ~ a polyfluoro metal or metalloid salt } of an alkali or alkaline earth metal to produce the desired arylalkyliodonium polyfluoro metal or metalloid salt , such as dimedonylphenyliodonium hexafluoroarsenate
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