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Caffeine by Starbucks Decaf Coffee Cup Size. The above amounts are posted by Starbucks, however, other independent tests found different results. Tests undertaken by the University of Florida showed that a 16oz serving of decaffeinated brewed coffee had caffeine concentrations of 12 to 13.4 milligrams.
Caffeine was isolated from the coffee samples and measured by gas chromatography. Every serving but one - instant decaffeinated Folgers Coffee Crystals - contained caffeine, ranging from 8.6 milligrams to 13.9 milligrams. In comparison, an 8-ounce cup of drip-brewed coffee typically contains 85 milligrams of caffeine. In the study's second phase, scientists analyzed 12 samples of Starbucks decaffeinated espresso and brewed decaffeinated coffee taken from a single store.