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1 Freeze drying or lyophilization is a drying method where the solvent is frozen prior to drying and is then sublimed, i.e., passed to the gas phase directly from the solid phase, below the melting point of the solvent.
separate, unique, and interdependent processes; freezing, primary drying (sublimation of ice at high. vacuum & at low temp), and secondary drying. (desorption water at low vacuum & at a temperature. above freezing point).2-7. It is a GMP integrated fundamental process in the. biopharmaceutical industry.