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Water is separated from the first overhead stream, and the resulting isobutylene-enriched stream is recycled back to the reaction step. The first bottoms stream is distilled to produce a bottoms product stream comprising diisobutylene and a second overhead stream comprising tertiary butyl alcohol and diisobutylene.he reaction product stream, comprising diisobutylene, isobutylene, TBA, and water, is purified by a process a shown in. . The reaction product stream is passed via line 11 to a first distillation tower 10. Tower 10 contains 35 ideal stages, 11 above feed and 24 below feed.
Patents. A process for preparing low molecular weight, highly reactive polyisobutylene having an average molecular weight Mn of from 500 to 5000 Dalton and a terminal double bond content of more than 80 mol % by polymerization in the liquid phase of isobutene or hydrocarbon streams comprising isobutane [sic]...ccording to stage (c) the enriched and/or separated catalyst complex is then recycled, usually without further purification, to the polymerization, in the case of a multi-stage polymerization generally into the first stage. It is generally possible to recycle from 70 to 90% of the catalyst complex.