 
  
 ICS 73.020; 91.100.15  
 
Reference number
DRS 541: 2023
© RSB 2023
  
 RWANDA 
STANDARD  DRS 
541 
 
First edition  
2023-mm-dd  
 
Natural stone test methods — 
Determination of resistance to ageing by 
thermal shock  
   
DRS 541: 2023 
©RSB 2023- All rights reserved                  ii 
 In order to match with technological development and to keep continuous progress in industries, 
standards are subject to periodic review. Users shall ascertain that they are in possession of the latest 
edition 
 
 
 
 
 
 
 
 
© RSB2023 
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized 
in any form or by any means, electronic or mechanical, including photocopying and microfilm, without 
prior written permission from RSB. 
Requests for permission to reproduce this document should be addressed to: 
Rwanda Standards Board 
P.O Box 7099 Kigali-Rwanda 
KK 15 Rd, 49 
Tel. +250 788303492 
Toll Free: 3250 
E-mail: info@rsb.gov.rw  
Website: www.rsb.gov.rw  
ePortal: www.portal.rsb.gov.rw  DRS 541: 2023 
iii                ©RSB 2023- All rights reserved 
 Contents Page 
Foreword ............................................................................................................................................................ iv  
1 Scope ...................................................................................................................................................... 1  
2 Normative references ............................................................................................................................ 1  
3 Terms and definitions ........................................................................................................................... 1  
4 Symbols (and abbreviated terms) ........................................................................................................ 1  
5 Principal ................................................................................................................................................. 2  
6 Apparatus ............................................................................................................................................... 2  
7 Preparation of specimens .................................................................................................................... 2  
7.1 Sampling ................................................................................................................................................ 2  
7.2 Dimensions of the test specimens ...................................................................................................... 2  
7.3 Putting reference marks on the specimens ........................................................................................ 3  
7.4 Drying the specimens ........................................................................................................................... 3  
8 Test procedure ....................................................................................................................................... 3  
8.1 Control measurements before cycling ................................................................................................ 3  
8.2 Description of the cycles ...................................................................................................................... 3  
8.3 Control measurements after cycling ................................................................................................... 3  
9 Expression of results ............................................................................................................................ 4  
9.1 Visual appearance ................................................................................................................................. 4  
9.2 Modulus of elasticity ............................................................................................................................. 4  
9.3 Open porosity ........................................................................................................................................ 4  
9.4 Ultrasound pulse velocity ..................................................................................................................... 4  
9.5 Flexural strength ................................................................................................................................... 4  
10 Test report .............................................................................................................................................. 5  
Annex A (normative)  Determination of sound speed propagation .............................................................. 7  
A.1 General ................................................................................................................................................... 7  
A.2 Determination of Pulse Velocity .......................................................................................................... 7  
A.2.1 Factors influencing pulse velocity measurements ............................................................................ 7  
A.2.2 Transducer arrangement ...................................................................................................................... 7  
A.2.3 Path length measurement .................................................................................................................... 8  
A.2.4 Coupling the transducer onto the stone ............................................................................................. 8  
A.2.5 Measurement of the transit time .......................................................................................................... 8  
A.3 Expression of the results ..................................................................................................................... 8  
 DRS 541: 2023 
©RSB 2023- All rights reserved                  iv 
 Foreword 
Rwanda Standardsarepreparedby Technical Committees and approved by Rwanda Standards Board (RSB) 
Board of Directors in accordance with the procedures of RSB, in compliance with Annex 3 of the WTO/TBT 
agreement on the preparation, adoption and application of standards. 
The main task of technical committees is to prepare national standards. Final Draft Rwanda Standards 
adopted by Technical committees are ratified by members of RSB Board of Directors for publication and 
gazettment as Rwanda Standards. 
DRS541was prepared by Technical Committee RSB/TC 9, Civil engineering and building materials  
In the preparation of this standard, reference was made to the following standard: 
1. BS EN 14066:2013: Natural stone test methods — Determination of resistance to ageing by thermal 
shock 
2. EN 14146, Natural stone test methods – Determination of the dynamic modulus of elasticity (by 
measuring the fundamental resonance frequency)  
 
The assistance derived from the above source is hereby acknowledged with thanks. 
DRS541 consists of the following parts, under the general title Natural stone test methods— Determination of 
resistance to ageing by thermal shock  
Committee membership  
The following organizations were represented on the Technical Committee on Civil engineering and building 
materials (RSB/TC 9) in the preparation of this standard. 
A+Construction Group Ltd 
Africeramics Ltd 
Consultants Engineers Group (CEG) Ltd 
D&D Resources Ltd 
Dutureheza Ltd 
Enabel Rwanda 
Greenpack Africa Ltd DRS 541: 2023 
v                ©RSB 2023- All rights reserved 
 Integrated Polytechnic Regional Centre (IPRC) - Musanze  
Mass Design Group 
NP Construction Company (NPCC) Ltd 
Road Transport Development Agency (RTDA) 
Rwanda Housing Authority (RHA) 
Rwanda Inspectorate, Competition and Consumer Protection Authority (RICA) 
Rwanda Quarries Association (RQA) 
SKAT Consult  
St Joseph Engineering Company (SJEC) Ltd 
Standards for Sustainability (SfS) 
Stonecraft Industries Ltd 
University of Rwanda - College of Science and Technology (UR - CST) 
Rwanda Standards Board (RSB) – Secretariat 
  DRS 541: 2023 
©RSB 2023- All rights reserved                  vi 
  DRS 541: 2023 
1                ©RSB 2023- All rights reserved 
 Natural stone test methods — Determination of resistance to ageing by 
thermal shock 
1 Scope 
This Draft Rwanda standard specifies a method to assess possible changes of natural stones under the effect 
of sudden changes in temperature (thermal shock). 
2 Normative references 
The following documents are referred to in the text in such a way that some or all of their content constitutes 
requirements of this document. For dated references, only the edition cited applies. For undated references, 
the latest edition of the referenced document (including any amendments) applies. 
DRS 526  Natural stone test methods – Determination of real density and apparent density, and of total and 
open porosity  
DRS 533 , Natural stone test methods – Determination of flexural strength under concentrated load  
DRS 515, Natural stone – Terminology 
3 Terms and definitions 
For the purposes of this standard, the terms and definitions in DRS 515  apply. 
4 Symbols (and abbreviated terms) 
Fr      Flexural strength tested on the reference specimens, in MPa  
Ff      Flexural strength tested on the specimens subjected to thermal cycles, in MPa  
∆F     Change in flexural strength between reference and exposed specimens, in %  
E0     Dynamic elastic modulus of the specimens before the thermal cycles, in MPa  
Ef     Dynamic elastic modulus of the specimens after the thermal cycles, in MPa  
∆E     Change in dynamic elastic modulus of the specimen, in %  
ρ0      Open porosity before the test, in %  
ρf      Open porosity after the test, in %   
©RSB 2023- All rights reserved                  2 
 ∆ρ -   Change in open porosity of the specimen, in %  
v0     Ultrasound pulse velocity (UPV) before the test, in km/s  
vf      Ultrasound pulse velocity (UPV) after the test, in km/s  
∆v     Change in Ultrasound pulse velocity of the specimen, in % 
5 Principal 
After drying at (40 ± 5) °C for a week, the specimens are subjected to successive cycles, each formed by 
drying at (70 ± 5) °C followed by immediate immersion in water at (20 ± 5) °C.  
The potential strength loss is measured according to DRS 533 . Exposed specimens and, when relevant, 
changes in other physical and mechanical properties are measured by one or more of the following non-
destructive tests: UPV (v0) according to Annex A , and open porosity (ρ0) according to DRS 526  , performed 
on specimens before and after the thermal cycles. 
6 Apparatus 
6.1 A ventilated oven capable of maintaining a temperature of (70 ± 5) °C.  
6.2 A covered tank with a flat base, comprising small non-oxidising and non-absorbent supports for the 
specimens.  
6.3 A weighing instrument with an accuracy of at least 0,01 % of the mass to be weighed.  
7 Preparation of specimens 
7.1 Sampling 
The sampling is not the responsibility of the test laboratory except where specially requested.  
At least 20 specimens shall be selected from a homogeneous batch: a set of 10 specimens as references for 
flexural strength measurement of fresh material and the other set for the thermal cycles.  
7.2 Dimensions of the test specimens 
The dimensions of the specimens shall be in accordance with DRS 533, i.e. determined by their thickness.  
 the thickness shall be between 25 mm and 100 mm and shall be greater than twice the size of the largest 
grain in the stone;  
 the total length shall be equal to six times the thickness;  
 the distance between the supporting rollers shall be equal to five times the thickness;  DRS 541: 2023 
3                ©RSB 2023- All rights reserved 
  the width shall be between 50 mm and three times the thickness and in no case shall it be less than the 
thickness.  
7.3 Putting reference marks on the specimens 
To ensure that the measurements of the dynamic elastic modulus or of the ultrasound pulse velocity 
performed before and after the thermal shock test are done at the same points, indelible marks in the form of 
points are made on the relevant faces of the specimens, to show the location of emitter and receiver.  
Indelible lines are traced to show the location of the axis of the two supports on which the specimens will be 
placed during the determination of the dynamic elastic modulus and the UPV. 
7.4 Drying the specimens 
The specimens are dried in a ventilated oven at (40 ± 5) °C for one week and then cooled to ambient 
temperature (20 ± 5) °C before start of the cycles.  
8 Test procedure 
8.1 Control measurements before cycling 
Before cycling, depending on the test chosen to evaluate the change in performance, the specimens 
subjected to cycles are measured according to one or more of the non-destructive tests:, UPV (v0) according 
to Annex A , and open porosity (ρ0) according to DRS 526.  
8.2 Description of the cycles 
The dried specimens are subjected to changes of temperature according to the following procedure: (18 ± 1) h 
in a ventilated oven at (70 ± 5) °C; immediately followed by (6 ± 0,5) h completely submerged in tap water, 
whose temperature before the immersion of the specimens is (20 ± 5) °C.  
Both in the oven and in the water container, the specimens are placed on the supports at a distance of at least 
50 mm from one another and from the wall. In the water container, the specimens are placed on supports 
located at the bottom of the container which has been filled with tap water to such a height that the water level 
above the specimens is (60 ± 10) mm. The procedure described above constitutes one cycle. If the test is to 
be interrupted at any time, other than for testing, then the specimens are to be immersed in water at (20 ± 5) 
°C.  
8.3 Control measurements after cycling 
After the 20th cycle, the specimens are dried to constant mass at (70 ± 5) °C. Constant mass is reached when 
the difference between two weighing at an interval of (24 ± 2) h is not greater than 0,1 % of the first of the two 
masses. Then they are visually inspected and compared with the reference specimens. All alterations are 
recorded.  
One or more of the non-destructive tests are performed: the UPV (vf) according to Annex A , and/or the open 
porosity (ρf) according to DRS 526 .   
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 Finally, the flexural strength test is performed according to DRS 533 , on the dried references specimens and 
on the specimens subjected to thermal cycles.  
9 Expression of results 
9.1 Visual appearance 
Describe the modifications observed visually by comparison with the reference specimen, such as:  
 cracking;  
 scaling or exfoliation.  
9.2 Modulus of elasticity 
Calculate the change in dynamic elastic modulus to the nearest 0,1 % according to Formula (1): 
∆𝐸=𝐸௙−𝐸௢
𝐸௢𝑥100 
9.3 Open porosity 
Calculate the change in open porosity to the nearest 0,1 % according to Formula (2):  
∆𝜌=𝜌௙−𝜌௢
𝜌௢𝑥100 
9.4 Ultrasound pulse velocity 
Calculate the change in ultrasound pulse velocity to the nearest 0,1 % according to Formula (3):  
 
∆𝑉=𝑉௙−𝑉௢
𝑉௢𝑥100 
9.5 Flexural strength 
Measure the flexural strength on dried reference and exposed specimens. The percentage change in flexural 
strength (ΔF) is calculated as follows:  
∆𝐸=𝐸௙−𝐸௥
𝐸௥𝑥100 DRS 541: 2023 
5                ©RSB 2023- All rights reserved 
 10 Test report 
The test report shall contain the following information:  
a) unique identification number of this report,  
b) the number, title and date of issue of this Rwanda  Standard;  
c) the name and address of the test laboratory and the address where the test was carried out if it is 
different from the test laboratory;  
d) the name and address of the client;  
e) it is the responsibility of the client to give the following information:  
1) the petrographic name of the stone;  
2) the commercial name of the stone;  
3) the country and region of extraction;  
4) the name of the supplier;  
5) the direction of any existing plane of anisotropy (if relevant to the test) to be clearly indicated on the 
sample or on each specimen by means of two parallel lines;  
6) the name of the person or organisation which carried out the sampling; 
7) the surface finish of the specimen (if relevant to the test).  
f) the date of delivery of the sample or of the specimens;  
g) the date when the specimens were prepared (if relevant) and the date of testing;  
h) the number of specimens in the sample;  
i) the dimensions of the specimens;  
j) any observed alteration for each specimen;  
k) the percentage change in dynamic elastic modulus for each specimen and the mean percentage change 
in dynamic elastic modulus (if performed);  
l) the percentage change in UPV for each specimen and the mean (if performed);   
©RSB 2023- All rights reserved                  6 
 m) the percentage change in open porosity for each specimen and the mean (if performed);  
n) the mean percentage change in flexural strength;  
o) a statement on measurement uncertainty (where appropriate);  
p) any deviations from the standard and their justification;  
q) remarks.  
The test report shall contain the signature(s) and role(s) of the responsible(s) for the testing and the date of 
issue of the report.  
It shall also state that the report shall not be partially reproduced without the written consent of the test 
laboratory. 
 
 
 
 
 
 
 
 
 
 
 
 
 
 DRS 541: 2023 
7                ©RSB 2023- All rights reserved Annex A 
(normative)  
 
Determination of sound speed propagation 
A.1 General 
The apparatus shall be used within the operating conditions stated by the manufacturer.  
A.2 Determination of Pulse Velocity 
A.2.1 Factors influencing pulse velocity measurements 
In order to provide a measurement of pulse velocity which is reproducible, it is necessary to take into account 
various factors which can influence the measurements. These are set out in informative Annex B.  
A.2.2 Transducer arrangement 
Although the direction in which the maximum energy is propagated is at right angles to the face of the 
transmitting transducer, it is possible to detect pulses which have travelled through the natural stone in some 
other direction. It is therefore possible to make measurements of pulse velocity by placing the two transducers 
either on opposite face (direct transmission), or on adjacent faces (semi-direct transmission), or on the same 
face (indirect or surface transmission). (see Figure 1).  
 
T = transmitter  
R = receiver  
a) direct transmission  
b) semi-direct transmission  
c) indirect or surface transmission  
 
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 Figure 1 — Different transducer arrangements for the determination of pulse velocity  
NOTE 1 It may be necessary to place the transducers on opposite faces but not directly opposite each other. Such 
arrangement shall be regarded as a semi-direct transmission. (see Figure 1.b).  
NOTE 2 The indirect transmission arrangement is the least sensitive and should only be used, for in situ measurements 
when only a single face of the natural stone is accessible, or when it is more important to determine the strength of the 
layer near the surface than that of the body of the stone itself.  
NOTE 3 The semi-direct transmission arrangement has a sensitivity intermediate between the other two arrangements 
and should only be used when the direct arrangement cannot be used.  
A.2.3 Path length measurement 
For direct transmission, the path length is the distance between the transducers measured with an accuracy of 
± 1 %.  
For semi-direct transmission, it is generally found to be sufficiently accurate to take the path length as the 
distance measured from centre to centre of the transducers faces. The accuracy of the measurement of the 
path length is dependent upon the size of the transducers compared with the centre to centre distance and it 
shall be estimated.  
With indirect transmission, the path length is not measured, but a series of measurements is made with the 
transducers at different distances apart.  
A.2.4 Coupling the transducer onto the stone 
There shall be adequate acoustical coupling between the stone and the face of each transducer. For 
sufficiently smooth surface finishes a good acoustical contact is ensured by the use of a coupling medium 
such as petroleum jelly, grease, soft soap and kaolin/glycerol paste and by pressing the transducer against 
the stone surface.  
Repeated readings of the transit time shall be made until a minimum value is obtained, so as to allow the layer 
of couplant to become thinly spread.  
When the surface finish is very rough and uneven, the surface area shall be smoothed and levelled by 
grinding, or by the use of a quick-setting epoxy resin.  
NOTE Special transducers are available for use on very rough surfaces  
A.2.5 Measurement of the transit time 
Using the electronic device the time interval indicated shall be recorded.  
A.3 Expression of the results 
For direct and semi-direct transmissions the pulse velocity shall be calculated from the formula:  DRS 541: 2023 
9                ©RSB 2023- All rights reserved 
 𝑉=𝐿
𝑇 
where 
V is the pulse velocity, in km/s  
L is the path length, in mm  
T is the time taken by the pulse to transverse the length, in µs  
For indirect transmission, the velocity shall be calculated in accordance with normative Annex A.  
The pulse velocity shall be expressed to the nearest 0,01 km/s.  
NOTE Recommendations on the procedures for correlating test results to compressive strength are given in EN 12504-4.  
©RSB 2023- All rights reserved                  10 
 Bibliography 
[1] DRS 5287, Natural stone test methods – Petrographic examination 
[2] EN 14146 Natural stone test methods Determination of the dynamic modulus of elasticity (by measuring 
the foundation resonance frequency) DRS 541: 2023 
 
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